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Painer, Florian; Drury, Martyn R; Hamers, Maartje F; Weikusat, Ilka (2026): Electron Backscatter Diffraction analysis on air hydrates of the EDML ice core [dataset]. PANGAEA, https://doi.pangaea.de/10.1594/PANGAEA.992544 (DOI registration in progress)

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Published: 2026-04-09

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Abstract:
In the deeper part of polar ice sheets, air hydrates are the primary air inclusions. They trap most of the ancient air molecules used for paleoclimatic reconstructions in their crystal structure. This dataset presents the first Electron Backscatter Diffraction (EBSD) measurements on air hydrates included in the EDML ice core. The sample was originally located at 2045.3 m depth. EBSD is a technique to characterize the microstructure of materials, which includes the precise determination of crystallographic orientations of measured materials. The measurements were taken by Florian Painer, Martyn Drury and Maartje Hamers at the University of Utrecht. The aim was to investigate the crystallographic nature and measure the crystallographic orientation of air hydrates included in polar ice. We thank Eric Hellebrand and Erik Betz-Güttner for their support in operating the Cryo-SEM. Access to the Cryo-SEM at MINT-UU (Utrecht University) was provided by EPOS-NL Facility Access, supported by the Dutch Research Council (NWO).
Keyword(s):
air hydrates; Antarctica; Cryo-SEM; EBSD analysis; Ice core
Related to:
Weikusat, Ilka; de Winter, Niels J; Pennock, Gillian M; Hayles, Michael F; Schneijdenberg, Chris T W M; Drury, Martyn R (2011): Cryogenic EBSD on ice: preserving a stable surface in a low pressure SEM. Journal of Microscopy, 242(3), 295-310, https://doi.org/10.1111/j.1365-2818.2010.03471.x
Funding:
Horizon 2020 (H2020), grant/award no. 955750: Research and training network on understanding Deep icE corE Proxies to Infer past antarctiC climatE dynamics (DEEPICE)
Coverage:
Latitude: -75.002500 * Longitude: 0.068400
Date/Time Start: 2024-05-02T13:53:00 * Date/Time End: 2024-05-02T15:58:00
Minimum Elevation: 2891.7 m * Maximum Elevation: 2891.7 m
Event(s):
EDML (EPICA Dronning Maud Land, DML28C01_00) * Latitude: -75.002500 * Longitude: 0.068400 * Date/Time Start: 2001-01-10T00:00:00 * Date/Time End: 2006-01-17T00:00:00 * Elevation: 2891.7 m * Recovery: 2774.15 m * Campaign: EPICA-Campaigns * Basis: Kohnen Station * Method/Device: EPICA drill (EDRILL) * Comment: Elevation is given with reference to WGS84
Parameter(s):
#NameShort NameUnitPrincipal InvestigatorMethod/DeviceComment
1Sample code/labelSample labelPainer, Florian
2DATE/TIMEDate/TimePainer, FlorianGeocode
3Temperature, deviceT Device°CPainer, FlorianCryo Preparation System, Quorum Technologies, PP3010cold stage temperature of scanning electron microscope (SEM)
4ImageIMAGEPainer, FlorianScanning electron microscope (SEM), Zeiss, Gemini 450SEM image
5SiteSitePainer, FlorianAZtec software, Oxford InstrumentsEBSD site
6Point IDPoint IDPainer, FlorianAZtec software, Oxford InstrumentsEBSD point
7PhasePhasePainer, FlorianAZtec software, Oxford Instruments
8AngleAngledegPainer, FlorianAZtec software, Oxford InstrumentsEuler angle 1 (Z)
9AngleAngledegPainer, FlorianAZtec software, Oxford InstrumentsEuler angle 2 (X')
10AngleAngledegPainer, FlorianAZtec software, Oxford InstrumentsEuler angle 3 (Z'')
11ImageIMAGEPainer, FlorianAZtec software, Oxford InstrumentsEBSD pattern
12ImageIMAGEPainer, FlorianAZtec software, Oxford InstrumentsEBSD pattern indexed
13CommentCommentPainer, Florian
Status:
Curation Level: Enhanced curation (CurationLevelC)
Size:
373 data points

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