Adenaya, Adenike; Rios-Quintero, Ruben; Lara-Martín, Pablo A; Zumbika, Florence; Wurl, Oliver; Ribas-Ribas, Mariana; Hamprecht, Axel; Brinkhoff, Thorsten: Analysis of antibiotics in environmental samples [dataset]. PANGAEA, https://doi.pangaea.de/10.1594/PANGAEA.974343 (dataset in review), In: Adenaya, A et al.: High concentrations of ciprofloxacin reduced bacterial abundance and enrichment in the sea surface microlayer (SML) and underlying water (ULW) and exerted selective pressure on marine bacteria [dataset bundled publication]. PANGAEA, https://doi.pangaea.de/10.1594/PANGAEA.974345 (dataset in review)
Abstract:
Due to its location at the air-sea interface, the sea surface microlayer is prone to accumulating anthropogenic pollutants. We analyzed the presence of antibiotic compounds, including ciprofloxacin, in this area using ultra-performance liquid chromatography—triple quadrupole mass spectrometry in tandem with ionization spray (UPLC-QqQMS/MS) (Bruker EVOQ Elite system, Billerica MA). We compared the numbers and concentrations of these compounds in the microlayer to those found in the underlying water column.
Keyword(s):
Funding:
German Research Foundation (DFG), grant/award no. 451574234: FOR 5267 - Biogeochemical processes and Air-sea exchange in the Sea-Surface microlayer (BASS)
Coverage:
Latitude: 53.533743 * Longitude: 8.183051
Date/Time Start: 2023-03-12T07:12:00 * Date/Time End: 2023-03-12T07:24:00
Minimum DEPTH, water: 0 m * Maximum DEPTH, water: 1 m
Event(s):
Jade_Bay-1 * Latitude: 53.533743 * Longitude: 8.183051 * Date/Time Start: 2023-03-17T08:00:00 * Date/Time End: 2023-03-17T10:00:00 * Location: Jade Bay, Wilhelshaven, Germany * Method/Device: Experiment (EXP) * Comment: Water tide depth: < 1 m. Device: Glass plate
Comment:
The value <0.001 in the data table refers to 'below the detection limit'. The specific limit of quantification for each antibiotic compound can be found in the supplementary information.
Parameter(s):
| # | Name | Short Name | Unit | Principal Investigator | Method/Device | Comment |
|---|---|---|---|---|---|---|
| 1 | Event label | Event | Adenaya, Adenike | |||
| 2 | DATE/TIME | Date/Time | Adenaya, Adenike | Geocode | ||
| 3 | Salinity, absolute | ASAL | g/kg | Adenaya, Adenike | ||
| 4 | Temperature, sample | T sample | °C | Adenaya, Adenike | ||
| 5 | pH | pH | Adenaya, Adenike | |||
| 6 | DEPTH, water | Depth water | m | Adenaya, Adenike | Geocode | |
| 7 | Device type | Device | Adenaya, Adenike | |||
| 8 | Sample type | Samp type | Adenaya, Adenike | |||
| 9 | Temperature, device | T Device | °C | Adenaya, Adenike | Storage Temperature | |
| 10 | Lincomycin | Lincomycin | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 11 | Clindamycin | Clindamycin | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 12 | Clarithromycin | Clarithromycin | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 13 | Spiramycin | Spiramycin | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 14 | Tylosin | Tylosin | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 15 | Erythromycin | Erythromycin | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 16 | Azithromycin | Azithromycin | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 17 | Ofloxacin | Ofloxacin | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 18 | Enrofloxacin | Enrofloxacin | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 19 | Roxithromycin | Roxithromycin | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 20 | Ciprofloxacin | Ciprofloxacin | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 21 | Sparfloxacin | Sparfloxacin | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 22 | Chloramphenicol | Chloramphenicol | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 23 | Sulfadiazine | Sulfadiazine | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 24 | Sulfadimethoxine | Sulfadimethoxine | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 25 | Sulfamethazine | Sulfamethazine | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 26 | Sulfamethizole | Sulfamethizole | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 27 | Sulfamethoxazole | Sulfamethoxazole | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 28 | Sulfaguanidine | Sulfaguanidine | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 29 | Sulfathiazole | Sulfathiazole | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 30 | Novobiocin | Novobiocin | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 31 | Doxycycline | Doxycycline | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 32 | Chlortetracycline | Chlortetracycline | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 33 | Oxytetracycline | Oxytetracycline | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 34 | Trimethoprim | Trimethoprim | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system | |
| 35 | Rifampicin | Rifampicin | ng/l | Adenaya, Adenike | Ultra-performance liquid chromatography - triple quadrupole mass spectrometry, (UPLC-QqQMS/MS), Bruker, EVOQ Elite system |
License:
Creative Commons Attribution 4.0 International (CC-BY-4.0) (License comes into effect after moratorium ends)
Status:
Curation Level: Enhanced curation (CurationLevelC)
Size:
128 data points