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Felden, Janine; Boetius, Antje (2013): Pore water geochemistry of Håkon Mosby mud volcano sediments measured at station PS74/168-1 (Sample 2, new flow surface) [dataset]. Max-Planck-Institut für Marine Mikrobiologie, PANGAEA, https://doi.org/10.1594/PANGAEA.810918, In supplement to: Ruff, S Emil; Felden, Janine; Gruber-Vodicka, Harald R; Marcon, Yann; Knittel, Katrin; Ramette, Alban; Boetius, Antje (2018): In situ development of a methanotrophic microbiome in deep-sea sediments. The ISME Journal, https://doi.org/10.1038/s41396-018-0263-1

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Abstract:
Pore water and turnover rates were determined for surface sediment cores obtained in 2009 and 2010. The pore water was extracted with Rhizons (Rhizon CSS: length 5 cm, pore diameter 0.15 µm; Rhizosphere Research Products, Wageningen, Netherlands) in 1 cm-resolution and immediately fixed in 5% zinc acetate (ZnAc) solution for sulfate, and sulfide analyses. The samples were diluted, filtered and the concentrations measured with non-suppressed anion exchange chromatography (Waters IC-Pak anion exchange column, waters 430 conductivity detector). The total sulfide concentrations (H2S + HS- + S**2-) were determined using the diamine complexation method (doi:10.4319/lo.1969.14.3.0454). Samples for dissolved inorganic carbon (DIC) and alkalinity measurements were preserved by adding 2 µl saturated mercury chloride (HgCl2) solution and stored headspace-free in gas-tight glass vials. DIC and alkalinity were measured using the flow injection method (detector VWR scientific model 1054) (doi:10.4319/lo.1992.37.5.1113). Dissolved sulfide was eliminated prior to the DIC measurement by adding 0.5 M molybdate solution (doi:10.4319/lo.1995.40.5.1011). Nutrient subsamples (10 - 15 ml) were stored at – 20 °C prior to concentration measurements with a Skalar Continuous-Flow Analyzer (doi:10.1002/9783527613984).
Funding:
Seventh Framework Programme (FP7), grant/award no. 226354: Hotspot Ecosystem Research and Mans Impact On European Seas
Sixth Framework Programme (FP6), grant/award no. 36851: European Seafloor Observatory Network
Coverage:
Latitude: 72.004700 * Longitude: 14.724200
Date/Time Start: 2009-07-23T13:49:00 * Date/Time End: 2009-07-23T13:49:00
Minimum DEPTH, sediment/rock: 0.005 m * Maximum DEPTH, sediment/rock: 0.290 m
Event(s):
PS74/168-1 * Latitude: 72.004700 * Longitude: 14.724200 * Date/Time: 2009-07-23T13:49:00 * Elevation: -1284.6 m * Location: Norwegian Sea * Campaign: ARK-XXIV/2 (PS74) * Basis: Polarstern * Method/Device: MultiCorer (MUC)
Parameter(s):
#NameShort NameUnitPrincipal InvestigatorMethod/DeviceComment
DEPTH, sediment/rockDepth sedmGeocode
SulfideS2-µmol/lFelden, JaninePhotometer, methylene blue (Cline 1969)
Sulfate[SO4]2-mmol/lFelden, JanineIon chromatography
Carbon, inorganic, dissolvedDICmmol/lFelden, JanineFlow injection analysis (Hall and Aller 1992)CO2 + HCO3- + CO32-
Alkalinity, totalATmmol(eq)/lFelden, JanineTwo-point titration (Edmond 1970)
SilicateSi(OH)4µmol/lFelden, JanineSeawater analysis after Grasshoff et al., 1983 (Verlag Chemie GmbH Weinheim)
Phosphate[PO4]3-µmol/lFelden, JanineSeawater analysis after Grasshoff et al., 1983 (Verlag Chemie GmbH Weinheim)
Ammonium[NH4]+µmol/lFelden, JanineSeawater analysis after Grasshoff et al., 1983 (Verlag Chemie GmbH Weinheim)
Size:
139 data points

Data

Download dataset as tab-delimited text — use the following character encoding:


Depth sed [m]

S2- [µmol/l]

[SO4]2- [mmol/l]

DIC [mmol/l]

AT [mmol(eq)/l]

Si(OH)4 [µmol/l]

[PO4]3- [µmol/l]

[NH4]+ [µmol/l]
0.0053521.850.99.111911332
0.0153517.841.212.112711760
0.0254011.321.651.111722121
0.035439.551.655.026932832
0.045436.891.861.133793260
0.055424.102.265.029343011
0.065403.442.264.437063244
0.075392.632.336.727542889
0.085422.712.438.342183376
0.095402.022.337.8336123295
0.110661.212.542.2376113007
0.130520.672.541.729782943
0.150420.512.540.634462427
0.170440.392.629.238572971
0.190432.526.529452968
0.210420.172.527.432462915
0.230380.152.424.238052955
0.250390.142.427.435953066
0.270370.112.625.318922825
0.290410.062.626.921042792