/* DATA DESCRIPTION: Citation: Felden, Janine; Boetius, Antje (2013): Pore water geochemistry of Håkon Mosby mud volcano sediments measured at station PS74/168-1 (Sample 2, new flow surface). Max-Planck-Institut für Marine Mikrobiologie, PANGAEA, https://doi.org/10.1594/PANGAEA.810918, In supplement to: Ruff, S Emil; Felden, Janine; Gruber-Vodicka, Harald R; Marcon, Yann; Knittel, Katrin; Ramette, Alban; Boetius, Antje (2018): In situ development of a methanotrophic microbiome in deep-sea sediments. The ISME Journal, https://doi.org/10.1038/s41396-018-0263-1 Abstract: Pore water and turnover rates were determined for surface sediment cores obtained in 2009 and 2010. The pore water was extracted with Rhizons (Rhizon CSS: length 5 cm, pore diameter 0.15 µm; Rhizosphere Research Products, Wageningen, Netherlands) in 1 cm-resolution and immediately fixed in 5% zinc acetate (ZnAc) solution for sulfate, and sulfide analyses. The samples were diluted, filtered and the concentrations measured with non-suppressed anion exchange chromatography (Waters IC-Pak anion exchange column, waters 430 conductivity detector). The total sulfide concentrations (H2S + HS- + S**2-) were determined using the diamine complexation method (doi:10.4319/lo.1969.14.3.0454). Samples for dissolved inorganic carbon (DIC) and alkalinity measurements were preserved by adding 2 µl saturated mercury chloride (HgCl2) solution and stored headspace-free in gas-tight glass vials. DIC and alkalinity were measured using the flow injection method (detector VWR scientific model 1054) (doi:10.4319/lo.1992.37.5.1113). Dissolved sulfide was eliminated prior to the DIC measurement by adding 0.5 M molybdate solution (doi:10.4319/lo.1995.40.5.1011). Nutrient subsamples (10 - 15 ml) were stored at – 20 °C prior to concentration measurements with a Skalar Continuous-Flow Analyzer (doi:10.1002/9783527613984). Project(s): European Seafloor Observatory Network (ESONET) (URI: https://cordis.europa.eu/project/id/36851) Hotspot Ecosystem Research and Mans Impact On European Seas (HERMIONE) (URI: https://www.eu-hermione.net/) Funding: Seventh Framework Programme (FP7), grant/award no. 226354: Hotspot Ecosystem Research and Mans Impact On European Seas (URI: https://cordis.europa.eu/project/id/226354) Sixth Framework Programme (FP6), grant/award no. 36851: European Seafloor Observatory Network (URI: https://cordis.europa.eu/project/id/36851) Coverage: LATITUDE: 72.004700 * LONGITUDE: 14.724200 DATE/TIME START: 2009-07-23T13:49:00 * DATE/TIME END: 2009-07-23T13:49:00 MINIMUM DEPTH, sediment/rock: 0.005 m * MAXIMUM DEPTH, sediment/rock: 0.290 m Event(s): PS74/168-1 * LATITUDE: 72.004700 * LONGITUDE: 14.724200 * DATE/TIME: 2009-07-23T13:49:00 * ELEVATION: -1284.6 m * LOCATION: Norwegian Sea * CAMPAIGN: ARK-XXIV/2 (PS74) (URI: https://doi.org/10.2312/BzPM_0607_2010) * BASIS: Polarstern (URI: https://doi.org/10.17815/jlsrf-3-163) * METHOD/DEVICE: MultiCorer (MUC) Parameter(s): DEPTH, sediment/rock [m] (Depth sed) * GEOCODE Sulfide [µmol/l] (S2-) * PI: Felden, Janine (https://orcid.org/0000-0002-4177-6644, janine.felden@awi.de, https://www.awi.de/en/about-us/organisation/staff/single-view/janine-felden.html) * METHOD/DEVICE: Photometer, methylene blue (Cline 1969) (URI: https://doi.org/10.4319/lo.1969.14.3.0454) Sulfate [mmol/l] ([SO4]2-) * PI: Felden, Janine (https://orcid.org/0000-0002-4177-6644, janine.felden@awi.de, https://www.awi.de/en/about-us/organisation/staff/single-view/janine-felden.html) * METHOD/DEVICE: Ion chromatography Carbon, inorganic, dissolved [mmol/l] (DIC) * PI: Felden, Janine (https://orcid.org/0000-0002-4177-6644, janine.felden@awi.de, https://www.awi.de/en/about-us/organisation/staff/single-view/janine-felden.html) * METHOD/DEVICE: Flow injection analysis (Hall and Aller 1992) (URI: https://doi.org/10.4319/lo.1992.37.5.1113) * COMMENT: CO2 + HCO3- + CO32- Alkalinity, total [mmol(eq)/l] (AT) * PI: Felden, Janine (https://orcid.org/0000-0002-4177-6644, janine.felden@awi.de, https://www.awi.de/en/about-us/organisation/staff/single-view/janine-felden.html) * METHOD/DEVICE: Two-point titration (Edmond 1970) (URI: https://doi.org/10.1016/0011-7471(70)90038-0) Silicate [µmol/l] (Si(OH)4) * PI: Felden, Janine (https://orcid.org/0000-0002-4177-6644, janine.felden@awi.de, https://www.awi.de/en/about-us/organisation/staff/single-view/janine-felden.html) * METHOD/DEVICE: Seawater analysis after Grasshoff et al., 1983 (Verlag Chemie GmbH Weinheim) Phosphate [µmol/l] ([PO4]3-) * PI: Felden, Janine (https://orcid.org/0000-0002-4177-6644, janine.felden@awi.de, https://www.awi.de/en/about-us/organisation/staff/single-view/janine-felden.html) * METHOD/DEVICE: Seawater analysis after Grasshoff et al., 1983 (Verlag Chemie GmbH Weinheim) Ammonium [µmol/l] ([NH4]+) * PI: Felden, Janine (https://orcid.org/0000-0002-4177-6644, janine.felden@awi.de, https://www.awi.de/en/about-us/organisation/staff/single-view/janine-felden.html) * METHOD/DEVICE: Seawater analysis after Grasshoff et al., 1983 (Verlag Chemie GmbH Weinheim) License: Creative Commons Attribution 3.0 Unported (CC-BY-3.0) (URI: https://creativecommons.org/licenses/by/3.0/) Size: 139 data points */ Depth sed [m] S2- [µmol/l] [SO4]2- [mmol/l] DIC [mmol/l] AT [mmol(eq)/l] Si(OH)4 [µmol/l] [PO4]3- [µmol/l] [NH4]+ [µmol/l] 0.005 35 21.85 0.9 9.1 119 1 1332 0.015 35 17.84 1.2 12.1 127 1 1760 0.025 40 11.32 1.6 51.1 117 2 2121 0.035 43 9.55 1.6 55.0 269 3 2832 0.045 43 6.89 1.8 61.1 337 9 3260 0.055 42 4.10 2.2 65.0 293 4 3011 0.065 40 3.44 2.2 64.4 370 6 3244 0.075 39 2.63 2.3 36.7 275 4 2889 0.085 42 2.71 2.4 38.3 421 8 3376 0.095 40 2.02 2.3 37.8 336 12 3295 0.110 66 1.21 2.5 42.2 376 11 3007 0.130 52 0.67 2.5 41.7 297 8 2943 0.150 42 0.51 2.5 40.6 344 6 2427 0.170 44 0.39 2.6 29.2 385 7 2971 0.190 43 2.5 26.5 294 5 2968 0.210 42 0.17 2.5 27.4 324 6 2915 0.230 38 0.15 2.4 24.2 380 5 2955 0.250 39 0.14 2.4 27.4 359 5 3066 0.270 37 0.11 2.6 25.3 189 2 2825 0.290 41 0.06 2.6 26.9 210 4 2792