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Peugeot, Christophe; Alexandre, Anne (2025): Soil water isotopes - extraction comparison [dataset]. PANGAEA, https://doi.pangaea.de/10.1594/PANGAEA.984875 (DOI registration in progress), In: Alexandre, Anne (2025): Climate and triple oxygen isotope of precipitation, groundwater, soil water, plant water, and phytolith data from West Africa (Benin and Senegal) [dataset bundled publication]. PANGAEA, https://doi.org/10.1594/PANGAEA.984133

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Published: 2025-11-24

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Abstract:
Triple oxygen and hydrogen isotope compositions of soil water from two cores sampled in Nalohou, Benin (loamy soil core NA-19-05-19) and Dahra, Senegal (sandy soil core DA-24-08-19). The soil waters were extracted by centrifugation and by cryogenic distillation, and analyzed by Cavity Ring Dow Spectroscopy (CRDS). The data have been used to compare the extraction technics.
Keyword(s):
phytolith; plant water; precipitation; soil water; triple oxygen isotopes; West Africa
Related to:
Alexandre, Anne; Outrequin, Clément; Vallet-Coulomb, Christine; Peugeot, Christophe; Grippa, Manuela; Aleman, Julie C; Voigt, Claudia; Landais, Amaëlle; Mougin, Eric; Ndiaye, Ousmane; Sonzogni, Corinne; Yang, David Au; Mazur, Jean-Charles; Couapel, Martine; Ogée, Jérôme; Ouani, Theodore; Afouda, Simon; Wubda, Maxime; Soumaguel, Nogmana; Houngnon, Alfred; Tagesson, Torbern; Fensholt, Rasmus (2025): What Does the Triple Isotopic Composition of Oxygen in Precipitation, Groundwater, Soil Water, Plant Water, and Phytoliths Reveal About Current and Past Hydrological Cycles? Journal of Geophysical Research: Biogeosciences, 130(10), e2024JG008615, https://doi.org/10.1029/2024JG008615
Source:
AMMA-CATCH (1999): Precipitation dataset (5 minutes rainfall), 30 long-term stations over the upper Oueme watershed (14 000 km2), Benin [dataset]. IRD, CNRS-INSU, OSUG, OMP, OREME, https://doi.org/10.17178/AMMA-CATCH.CL.RAIN_O
AMMA-CATCH (2005): Surface flux dataset (including meteorological data, radiative budget, surface energy, water vapor and carbon fluxes), within the Donga watershed (600 km2), Benin [dataset]. IRD, CNRS-INSU, OSUG, OMP, OREME, https://doi.org/10.17178/AMMA-CATCH.AE.H2OFLUX_ODC
Funding:
Agence Nationale de la Recherche (ANR), grant/award no. ANR-17-CE01-0002: Past dynamic of continental atmospheric humidity and vegetation: new insights from the triple isotopic composition of oxygen (HUMI-17)
Parameter(s):
#NameShort NameUnitPrincipal InvestigatorMethod/DeviceComment
CampaignCampaignPeugeot, Christophe
CommentCommentAlexandre, Anne
Area/localityAreaAlexandre, Anne
Sample code/labelSample labelAlexandre, Anne
Depth, soil, minimumDepth soil minmAlexandre, AnneSoil corer
Depth, soil, maximumDepth soil maxmAlexandre, AnneSoil corer
DEPTH, soilDepth soilmAlexandre, AnneSoil corerGeocode – Average
Water content, dry massWater dm%Alexandre, AnneOvenInitial
ExtractExtract%Alexandre, AnneCentrifugation and cryogenic distillationExtracted water (% initial water); cf Alexandre et al., (2025). JGR
10 Extraction methodExtractionAlexandre, AnneCentrifugation and cryogenic distillationcf Alexandre et al., (2025). JGR
11 LaboratoryLabAlexandre, Anne
12 δ'18O, soil waterδ'18O soil w‰ SMOWAlexandre, AnneCavity ring-down spectroscopy (CRDS)average, vs VSMOW
13 δ'18O, soil water, standard deviationδ'18O soil w std dev±Alexandre, AnneCavity ring-down spectroscopy (CRDS)
14 δ'17O, soil waterδ'17O soil w‰ SMOWAlexandre, AnneCavity ring-down spectroscopy (CRDS)average, vs VSMOW
15 δ'17O, soil water, standard deviationδ'17O soil w std dev±Alexandre, AnneCavity ring-down spectroscopy (CRDS)
16 Oxygen-17 excess, soil water17O xs soil wper megAlexandre, AnneCavity ring-down spectroscopy (CRDS)average
17 Oxygen-17 excess, soil water, standard deviation17O xs soil w std dev±Alexandre, AnneCavity ring-down spectroscopy (CRDS)
18 Deuterium excess, soil waterd xs soil wAlexandre, AnneCavity ring-down spectroscopy (CRDS)average
19 Deuterium excess, soil water, standard deviationd xs soil w std dev±Alexandre, AnneCavity ring-down spectroscopy (CRDS)
20 Δδ'18OΔδ'18OAlexandre, AnneCavity ring-down spectroscopy (CRDS)d'18O average: difference centrifugation-distillation
21 Δδ'17OΔδ'17OAlexandre, AnneCavity ring-down spectroscopy (CRDS)d'17O average: difference centrifugation-distillation
22 Δ Oxygen-17 excessΔ17O xsper megAlexandre, AnneCavity ring-down spectroscopy (CRDS)17O-excess average : difference centrifugation-distillation
23 Δ Deuterium excessΔd xsAlexandre, AnneCavity ring-down spectroscopy (CRDS)d-excess average : difference centrifugation-distillation
Status:
Curation Level: Enhanced curation (CurationLevelC)
Size:
387 data points

Data

Download dataset as tab-delimited text — use the following character encoding:


Campaign

Comment

Area

Sample label

Depth soil min [m]

Depth soil max [m]

Depth soil [m]

Water dm [%]

Extract [%]
10 
Extraction
11 
Lab
12 
δ'18O soil w [‰ SMOW]
13 
δ'18O soil w std dev [±]
14 
δ'17O soil w [‰ SMOW]
15 
δ'17O soil w std dev [±]
16 
17O xs soil w [per meg]
17 
17O xs soil w std dev [±]
18 
d xs soil w []
19 
d xs soil w std dev [±]
20 
Δδ'18O []
21 
Δδ'17O []
22 
Δ17O xs [per meg]
23 
Δd xs []
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonNalohou (Benin)NA-190519-A20.0000.1400.07038.0CentriCEREGE
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonNalohou (Benin)NA-190519-A30.1400.2600.200542.7CentriCEREGE-3.2870.071-1.7290.039654.700.660.800.41-7.920.54
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonNalohou (Benin)NA-190519-A40.2600.3800.320652.7CentriCEREGE-3.6030.057-1.8940.029937.220.600.720.37-8.070.14
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonNalohou (Benin)NA-190519-B20.3800.4700.425547.0CentriCEREGE-2.4090.070-1.2770.042-580.711.030.700.370.79-1.30
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonNalohou (Benin)NA-190519-B30.4700.5600.515549.2CentriCEREGE-2.0750.066-1.1090.042-13110.610.890.400.21-0.20-1.57
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonNalohou (Benin)NA-190519-B40.5600.6400.600333.3CentriCEREGE-1.5260.090-0.8300.049-252-4.761.121.520.79-9.95-7.95
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonNalohou (Benin)NA-190519-A20.0000.1400.0703100.0DistISPA-3.2640.010-1.7380.014-159-5.580.13
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonNalohou (Benin)NA-190519-A30.1400.2600.200598.0DistISPA-4.0870.007-2.1440.0021454.160.16
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonNalohou (Benin)NA-190519-A40.2600.3800.320699.0DistISPA-4.3190.008-2.2630.0081777.080.15
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonNalohou (Benin)NA-190519-B20.3800.4700.4255100.0DistISPA-3.1130.008-1.6500.006-642.010.15
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonNalohou (Benin)NA-190519-B30.4700.5600.5155101.0DistISPA-2.4740.017-1.3190.016-13132.180.20
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonNalohou (Benin)NA-190519-B40.5600.6400.6003100.0DistISPA-3.0490.028-1.6240.011-1593.190.40
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonDahra (Senegal)DAB-240819-P1-A20.0400.1330.087762.3CentriCEREGE-2.5810.099-1.3620.04616-1.521.260.66-0.422.69
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonDahra (Senegal)DAB-240819-P1-A30.1400.2400.1904100.0CentriCEREGE-2.9140.120-1.5300.0628101.711.870.630.349.500.96
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonDahra (Senegal)DAB-240819-P1-A40.2400.3200.2804100.0CentriCEREGE-3.1540.112-1.6540.0551153.971.580.120.074.782.29
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonDahra (Senegal)DAB-240819-P1-B20.3900.4730.432466.7CentriCEREGE-2.3520.141-1.2450.075-31-0.631.480.750.39-0.060.81
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonDahra (Senegal)DAB-240819-P1-A20.0400.1330.087798.0DistISPA-3.8390.013-2.0260.00319-4.210.29
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonDahra (Senegal)DAB-240819-P1-A30.1400.2400.1904100.0DistISPA-3.5470.013-1.8740.015-180.750.20
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonDahra (Senegal)DAB-240819-P1-A40.2400.3200.2804100.0DistISPA-3.2780.026-1.7240.013611.680.46
ANR HUMI-17 isotope monitoring in Benin and SenegalSoil water extraction comparisonDahra (Senegal)DAB-240819-P1-B20.3900.4730.432499.0DistISPA-3.0980.028-1.6390.019-35-1.440.56