Citation:

PANGAEA.969084

Name: Carbonates from Palouse loess at site CLY-2, eastern Washington, USA
Published: 2024-06-25
License: https://creativecommons.org/licenses/by/4.0/
Keywords: Loess; Magnetic susceptibility; paleoenvironment; paleosol; Palouse; Quaternary

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Published: 2024-06-25 • DOI registered: 2024-06-26

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Abstract:

These data are from samples gathered in 2016 from the CLY-2 site in eastern Washington, USA (Location: 46.3131, -118.4874, WGS84). The CLY-2 is a roadcut exposing a vertical face of the Palouse loess containing carbonate paleosol horizons and tephras. The samples were collected from a set of three stepped trenches into the roadcut about 10-20 m apart. Each trench was excavated to a depth of about a meter to expose a fresh surface; the final ~10 cm was excavated with non-ferrous digging tools.

Samples were analyzed for organic and inorganic carbon concentrations using an ECS 4010 Elemental Combustion Analyzer CNS (Costech Analytical Technologies, Valencia, CA) at the Arizona Laboratory for Emerging Contaminants. Each sample was ground in a Spex mill with tungsten carbide grind surfaces, then split into two aliquots; one aliquot was run to obtain total carbon, and the second was pretreated stepwise with HCl to remove inorganic C (Nelson and Sommers, 1996, doi:10.2136/sssabookser5.3.c34) before being run to obtain organic C. The difference between these aliquots is the reported inorganic C concentration. We assume all inorganic carbon is calcium carbonate, so CaCO3 is inorganic C multiplied by 8.3 to account for stoichiometric Ca and O.

Keyword(s):

Loess; Magnetic susceptibility; paleoenvironment; paleosol; Palouse; Quaternary

Supplement to:

Bader, Nicholas E; Broze, Elliot A; Coates, Molly A; Elliott, McKenzie M; McGann, Gabriella E; Strozyk, Sarah; Burmester, Russell F (in review): The magnetic susceptibility of the Quaternary Palouse loess, northwestern United States: implications for paleoclimate and stratigraphic studies. Quaternary International

References:

Nelson, D W; Sommers, L E (2018): Total Carbon, Organic Carbon, and Organic Matter. In: Sparks, DL, Page, AL, Helmke, PA, Loeppert, RH, Soltanpour, PN, Tabatabai, MA, Johnston, CT, Sumner, ME (eds.), Methods of Soil Analysis, SSSA Book Series, Soil Science Society of America, American Society of Agronomy, Madison, WI, USA, 961-1010, https://doi.org/10.2136/sssabookser5.3.c34

Funding:

M J Murdock Charitable Trust, grant/award no. 2015295: A record of Quaternary paleoclimate from the Palouse loess, southeastern Washington

Coverage:

Latitude: 46.313100 * Longitude: 118.487400

Date/Time Start: 2016-07-19T00:00:00 * Date/Time End: 2016-07-19T00:00:00

Event(s):

CLY-2 (ClydeSampling) * Latitude: 46.313100 * Longitude: 118.487400 * Date/Time: 2016-07-19T00:00:00 * Location: Washington, USA * Method/Device: Outcrop sample (OUTCROP) * Comment: Horizontal datum: WGS84, Vertical datum: NAVD88, Elevation of ground surface: 385 m, Elevation at outcrop base: 370 m

Parameter(s):

#	Name	Short Name	Unit	Principal Investigator	Method/Device	Comment
1	Sample ID	Sample ID		Bader, Nicholas E
2	Carbon, organic, total	TOC	%	Bader, Nicholas E	Elemental Analyser, COSTECH, ECS4010	wt%
3	Carbon, inorganic, total	TIC	%	Bader, Nicholas E	Elemental Analyser, COSTECH, ECS4010	wt %
4	Calcium carbonate, total	CaCO3 tot	%	Bader, Nicholas E	Elemental Analyser, COSTECH, ECS4010	Total carbonate [weight percent]

License:

Creative Commons Attribution 4.0 International (CC-BY-4.0)

Status:

Curation Level: Enhanced curation (CurationLevelC)

Size:

524 data points

Data

Download dataset as tab-delimited text — use the following character encoding:

1 Sample ID	2 TOC [%]	3 TIC [%]	4 CaCO3 tot [%]
15	0.05	0.13	1.08
20	0.08	0.25	2.08
25	0.10	0.44	3.67
30	0.11	0.33	2.75
35	0.09	0.47	3.92
40	0.09	0.52	4.37
45	0.12	1.11	9.25
50	0.14	1.43	11.92
55	0.11	1.14	9.50
60	0.11	1.17	9.75
65	0.11	1.12	9.29
70	0.47	0.96	8.00
75	0.22	1.29	10.75
80	0.15	1.16	9.67
85	0.11	1.17	9.75
90	0.10	1.13	9.42
95	0.07	1.16	9.67
100	0.08	0.94	7.83
105	0.09	1.01	8.42
110	0.10	1.00	8.37
115	0.09	1.02	8.50
120	0.33	0.77	6.42
125	0.36	0.87	7.25
130	0.13	0.50	4.17
135	0.12	1.09	9.08
140	0.14	1.19	9.92
145	0.43	0.80	6.67
150	0.31	1.02	8.50
155	0.10	0.60	5.00
160	0.08	0.57	4.75
165	0.07	0.69	5.75
170	0.09	0.86	7.17
175	0.15	0.70	5.83
180	0.06	0.91	7.58
185	0.16	1.02	8.50
190	0.08	0.81	6.75
195	0.08	0.70	5.83
200	0.07	0.72	6.00
205	0.06	0.83	6.92
210	0.06	0.94	7.83
215	0.06	0.32	2.67
220	0.12	0.30	2.50
225	0.12	0.36	3.00
230	0.16	0.55	4.58
235	0.14	0.76	6.37
240	0.17	1.10	9.17
245	0.14	0.73	6.08
250	0.12	0.76	6.33
255	0.17	0.59	4.92
260	0.09	0.23	1.92
265	0.09	0.20	1.67
270	0.11	0.52	4.33
275	0.09	0.38	3.17
280	0.08	0.48	3.96
285	0.08	0.24	2.00
290	0.09	0.20	1.67
295	0.09	0.36	3.00
300	0.08	0.19	1.58
305	0.08	0.14	1.17
310	0.08	0.06	0.50
315	0.15	0.71	5.92
320	0.14	0.67	5.58
325	0.12	0.45	3.75
330	0.12	0.42	3.50
335	0.16	1.20	10.00
340	0.13	0.50	4.17
345	0.13	0.53	4.42
350	0.11	0.55	4.58
355	0.12	0.65	5.42
360	0.11	0.66	5.50
365	0.12	0.47	3.92
370	0.11	0.86	7.17
375	0.11	0.70	5.83
380	0.12	0.66	5.50
385	0.12	0.68	5.67
390	0.12	0.84	7.00
395	0.11	0.82	6.83
400	0.15	0.95	7.92
405	0.22	0.38	3.17
410	0.23	0.94	7.83
415	0.11	0.92	7.67
420	0.14	1.00	8.33
425	0.11	0.85	7.08
430	0.09	0.41	3.42
435	0.13	1.04	8.67
440	0.12	0.80	6.71
445	0.13	0.78	6.50
450	0.12	0.65	5.42
455	0.12	0.39	3.25
460	0.12	0.41	3.42
465	0.10	0.27	2.25
470	0.11	0.55	4.58
475	0.10	0.51	4.25
480	0.10	0.47	3.92
485	0.10	0.45	3.75
490	0.13	0.49	4.08
495	0.05	0.33	2.75
500	0.06	0.17	1.42
505	0.22	0.14	1.17
510	0.19	0.82	6.83
515	0.15	0.06	0.50
520	0.20	0.04	0.33
525	0.21	0.04	0.33
530	0.28	0.02	0.17
535	0.39	0.05	0.42
540	0.60	0.10	0.83
545	0.61	0.09	0.75
550	0.05	0.15	1.25
555	0.05	0.22	1.83
560	0.04	0.15	1.25
565	0.06	0.28	2.33
570	0.06	0.29	2.42
575	0.06	0.25	2.08
580	0.06	0.24	2.00
585	0.07	0.31	2.58
590	0.13	0.29	2.42
595	0.06	0.23	1.92
600	0.11	0.31	2.58
605	0.14	0.28	2.33
610	0.17	0.35	2.92
615	0.07	0.19	1.58
620	0.07	0.35	2.92
625	0.06	0.36	3.00
630	0.05	0.51	4.25
635	0.08	0.83	6.92
640	0.08	1.03	8.58
645	0.07	0.82	6.83
650	0.07	0.97	8.08
655	0.06	0.79	6.58
665	0.05	0.59	4.92
670	0.06	0.63	5.25