Logemann, Anna Elisabeth; Röhrs, Steffen; Brockmeyer, Berit (2022): Determination of hydrophobic organic contaminants in sediment fines and bulk sediment [dataset]. PANGAEA, https://doi.org/10.1594/PANGAEA.950287
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Published: 2022-11-08 • DOI registered: 2023-01-09
Abstract:
We investigated 41 hydrophobic organic contaminants set of sediment samples (from 16 monitoring stations) taken in the North Sea (German EEZ). The samples were taken by the German Federal Maritime and Hydrographic Agency (BSH) in June 2016 on the RV Atair (Cruise AT239) using a box corer. Bulk sediment samples were analyzed for hydrophobic organic contaminants unsing micowave extraction, column clean-up, size-exclusion chromatography followed by GC-MS/MS analysis. Bulk sediment samples were additionally wet-sieved to seperate the sediment fine fraction (< 63 µm) which was analyzed accordingly. This study provides a comprehensive overview of hydrophobic organic contaminant concentrations in sediment fines (< 63 µm) for the German EEZ. The results indicate that the improved wet-sieving procedure is capable of physically normalizing the concentrations of the investigated contaminants and is useful for the comparison of different sediment types.
Related to:
Bundesanstalt für Gewässerkunde (2021): Meeresumweltdatenbank (MUDAB). Version 1.5.2 (13.08.2021). https://geoportal.bafg.de/MUDABAnwendung/
Witt, Gesine; Brockmeyer, Berit; Niehus, Nora Claire; Reininghaus, Mathias (2017): Organic contaminants (PAH, PCB and DDT) in sediments and porewater of the German Exclusive Economic Zone sampled in 2013/2014 [dataset]. Hochschule für Angewandte Wissenschaften Hamburg - Hamburg University of Applied Sciences and Bundesamt für Seeschiffahrt und Hydrographie, Hamburg, PANGAEA, https://doi.org/10.1594/PANGAEA.875181
Project(s):
Funding:
Federal Ministry of Education and Research (BMBF), grant/award no. 03F0669A: North Sea Observation and Assessment of Habitats
Coverage:
Median Latitude: 54.623444 * Median Longitude: 6.920513 * South-bound Latitude: 53.673300 * West-bound Longitude: 4.250000 * North-bound Latitude: 55.766700 * East-bound Longitude: 8.383300
Date/Time Start: 2016-05-24T11:10:00 * Date/Time End: 2016-05-31T16:15:00
Minimum DEPTH, sediment/rock: 0.02 m * Maximum DEPTH, sediment/rock: 0.02 m
Event(s):
AT239_BL4 * Latitude: 54.250000 * Longitude: 7.800000 * Date/Time: 2016-05-30T15:40:00 * Elevation: -27.0 m * Location: North Sea * Campaign: Atair239 (AT239) * Basis: Atair * Method/Device: Box corer (BC)
Parameter(s):
| # | Name | Short Name | Unit | Principal Investigator | Method/Device | Comment |
|---|---|---|---|---|---|---|
| 1 | Event label | Event | Logemann, Anna Elisabeth | |||
| 2 | Station label | Station | Logemann, Anna Elisabeth | |||
| 3 | Sample code/label | Sample label | Logemann, Anna Elisabeth | |||
| 4 | Elevation of event | Elevation | m | Logemann, Anna Elisabeth | ||
| 5 | DEPTH, sediment/rock | Depth sed | m | Logemann, Anna Elisabeth | Geocode | |
| 6 | Latitude of event | Latitude | Logemann, Anna Elisabeth | |||
| 7 | Longitude of event | Longitude | Logemann, Anna Elisabeth | |||
| 8 | DATE/TIME | Date/Time | Logemann, Anna Elisabeth | Geocode – UTC | ||
| 9 | Carbon, organic, total, per unit sediment mass | TOC/sed | mg/g | Logemann, Anna Elisabeth | Carbon and nitrogen and sulfur (CNS) isotope element analyzer, Elementar, Vario EL III | measured in sediment, grain size fraction <63 µm. The TOC analysis was carried out with a VarioEL (Elementar, Germany) in CN mode at 950 degC. The dried and homogenized samples were weighted in silver capsules, acidified with 200 microL of 2 M HCl (32%) and placed in an oven for 3 h at 110 degC to remove the inorganic carbon. |
| 10 | Acenaphthene, per unit sediment mass | Acenaphthene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.21 ng/g, limit of quantification: 0.56 ng/g |
| 11 | Acenaphthylene, per unit sediment mass | Acenaphthylene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.17 ng/g, limit of quantification: 0.45 ng/g |
| 12 | Anthracene, per unit sediment mass | Anthracene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.12 ng/g, limit of quantification: 0.33 ng/g |
| 13 | Benz(a)anthracene, per unit sediment mass | Benz(a)anthracene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.31 ng/g, limit of quantification: 0.79 ng/g |
| 14 | Benzo(a)pyrene, per unit sediment mass | Benzo(a)pyrene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.35 ng/g, limit of quantification: 0.91 ng/g |
| 15 | Benzo(b)fluoranthene, per unit sediment mass | Benzo(b)fluoranthene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.31 ng/g, limit of quantification: 0.80 ng/g |
| 16 | Benzo(g,h,i)perylene, per unit sediment mass | Benzo(g,h,i)perylene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.05 ng/g, limit of quantification: 0.15 ng/g |
| 17 | Chrysene/Triphenylene, per unit sediment mass | Chrysene/Triphenylene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.08 ng/g, limit of quantification: 0.20 ng/g |
| 18 | Dibenz(a,h)anthracene, per unit sediment mass | Dibenz(ah)anthracene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.29 ng/g, limit of quantification: 0.75 ng/g |
| 19 | Fluoranthene, per unit sediment mass | Fluoranthene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.11 ng/g, limit of quantification: 0.30 ng/g |
| 20 | Fluorene, per unit sediment mass | Fluorene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.18 ng/g, limit of quantification: 0.47 ng/g |
| 21 | Indeno(1,2,3-cd)pyrene, per unit sediment mass | Indeno(1,2,3-cd)pyr/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.33 ng/g, limit of quantification: 0.86 ng/g |
| 22 | Naphthalene, per unit sediment mass | Naphth/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.26 ng/g, limit of quantification: 0.50 ng/g |
| 23 | Phenanthrene, per unit sediment mass | Phenanthrene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.10 ng/g, limit of quantification: 0.28 ng/g |
| 24 | Pyrene, per unit sediment mass | Pyrene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.21 ng/g, limit of quantification: 0.55 ng/g |
| 25 | 1-Methylnaphthalene, per unit sediment mass | 1-Methylnaphthalene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.10 ng/g, limit of quantification: 0.28 ng/g |
| 26 | 2-Methylnaphthalene, per unit sediment mass | 2-Methylnaphthalene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.17 ng/g, limit of quantification: 0.44 ng/g |
| 27 | 3-Methylphenanthrene, per unit sediment mass | 3-Methylphenanthrene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.45 ng/g, limit of quantification: 1.2 ng/g |
| 28 | 2,6-Dimethylnaphthalene, per unit sediment mass | 2,6-Dimethylnaphthalene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.07 ng/g, limit of quantification: 0.19 ng/g |
| 29 | 3,6-Dimethylphenanthrene, per unit sediment mass | 3,6-Dimethylphenanthrene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.29 ng/g, limit of quantification: 0.77 ng/g |
| 30 | 2,3,5-Trimethylnaphthalene, per unit sediment mass | 2,3,5-Trimethylnaphthalene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.04 ng/g, limit of quantification: 0.10 ng/g |
| 31 | 1,2,8-Trimethylphenanthrene, per unit sediment mass | 1,2,8-Trimethylphenanthrene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.09 ng/g, limit of quantification: 0.24 ng/g |
| 32 | Dimethylated Naphthalenes, per unit sediment mass | Dimethylated Naphthalene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | sum, measured in sediment, grain size fraction <63 µm, limit of detection: 0.070 ng/g, limit of quantification: 0.19 ng/g |
| 33 | Trimethylated Naphthalenes, per unit sediment mass | Trimethylated Naphthalenes/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | sum, measured in sediment, grain size fraction <63 µm, limit of detection: 0.25 ng/g, limit of quantification: 0.64 ng/g |
| 34 | Methylated Phenantrenes, per unit sediment mass | Methylated Phenantrenes/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | sum, measured in sediment, grain size fraction <63 µm, limit of detection: 0.45 ng/g, limit of quantification: 1.2 ng/g |
| 35 | Dimethylated Phenantrenes, per unit sediment mass | Dimethylated Phenantrenes/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | sum, measured in sediment, grain size fraction <63 µm, limit of detection: 0.29 ng/g, limit of quantification: 0.76 ng/g |
| 36 | Trimethylated Phenantrenes, per unit sediment mass | Trimethylated Phenantrenes/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | sum, measured in sediment, grain size fraction <63 µm, limit of detection: 0.09 ng/g, limit of quantification: 0.24 ng/g |
| 37 | 2,4,4'-Trichlorobiphenyl, per unit sediment mass | 2,4,4-Trichlorobiphenyl/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.004 ng/g, limit of quantification: 0.01 ng/g |
| 38 | 2,2',5,5'-Tetrachlorobiphenyl, per unit sediment mass | C12H6Cl4/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.001 ng/g, limit of quantification: 0.002 ng/g |
| 39 | 2,2',4,5,5'-Pentachlorobiphenyl, per unit sediment mass | C12H5Cl5/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.005 ng/g, limit of quantification: 0.01 ng/g |
| 40 | 2,3',4,4,5'-Pentachlorobiphenyl, per unit sediment mass | 2,3',4,4,5'-Pentachlorobiphenyl/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.003 ng/g, limit of quantification: 0.007 ng/g |
| 41 | 2,2',3,4,4',5'-Hexachlorobiphenyl, per unit sediment mass | C12H4Cl6/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.002 ng/g, limit of quantification: 0.005 ng/g |
| 42 | 2,2',4,4',5,5'-Hexachlorobiphenyl, per unit sediment mass | C12H4Cl6/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.006 ng/g, limit of quantification: 0.01 ng/g |
| 43 | 2,2',3,4,4',5,5'-Heptachlorobiphenyl, per unit sediment mass | C12H3Cl7/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.005 ng/g, limit of quantification: 0.01 ng/g |
| 44 | alpha-Hexachlorocyclohexane, per unit sediment mass | a-HCH/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.01 ng/g, limit of quantification: 0.02 ng/g |
| 45 | beta-Hexachlorocyclohexane, per unit sediment mass | b-HCH/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.005 ng/g, limit of quantification: 0.01 ng/g |
| 46 | gamma-Hexachlorocyclohexane, per unit sediment mass | g-HCH/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.004 ng/g, limit of quantification: 0.01 ng/g |
| 47 | Hexachlorobenzene, per unit sediment mass | HCB/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.002 ng/g, limit of quantification: 0.006 ng/g |
| 48 | para,para-Dichlorodiphenyldichloroethane, per unit sediment mass | pp-DDD/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.007 ng/g, limit of quantification: 0.01 ng/g |
| 49 | para,para-Dichlorodiphenyldichloroethylene, per unit sediment mass | pp-DDE/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.002 ng/g, limit of quantification: 0.005 ng/g |
| 50 | para,para-Dichlorodiphenyltrichloroethane, per unit sediment mass | pp-DDT/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, grain size fraction <63 µm, limit of detection: 0.008 ng/g, limit of quantification: 0.01 ng/g |
| 51 | Carbon, organic, total, per unit sediment mass | TOC/sed | mg/g | Logemann, Anna Elisabeth | Carbon and nitrogen and sulfur (CNS) isotope element analyzer, Elementar, Vario EL III | measured in sediment, total. The TOC analysis was carried out with a VarioEL (Elementar, Germany) in CN mode at 950 degC. The dried and homogenized samples were weighted in silver capsules, acidified with 200 microL of 2 M HCl (32%) and placed in an oven for 3 h at 110 degC to remove the inorganic carbon. |
| 52 | Size fraction < 0.020 mm | <20 µm | % | Logemann, Anna Elisabeth | Laser Particle Analyser, Fritsch GmbH, Analysette 22 | measured in sediment, total |
| 53 | Size fraction < 0.063 mm, mud, silt+clay | <63 µm | % | Logemann, Anna Elisabeth | Laser Particle Analyser, Fritsch GmbH, Analysette 22 | measured in sediment, total |
| 54 | Size fraction < 0.200 mm | <200 µm | % | Logemann, Anna Elisabeth | Laser Particle Analyser, Fritsch GmbH, Analysette 22 | measured in sediment, total |
| 55 | Size fraction < 2.0 mm | <2000 µm | % | Logemann, Anna Elisabeth | Laser Particle Analyser, Fritsch GmbH, Analysette 22 | measured in sediment, total |
| 56 | Acenaphthene, per unit sediment mass | Acenaphthene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.21 ng/g, limit of quantification: 0.56 ng/g |
| 57 | Acenaphthylene, per unit sediment mass | Acenaphthylene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.17 ng/g, limit of quantification: 0.45 ng/g |
| 58 | Anthracene, per unit sediment mass | Anthracene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.12 ng/g, limit of quantification: 0.33 ng/g |
| 59 | Benz(a)anthracene, per unit sediment mass | Benz(a)anthracene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.31 ng/g, limit of quantification: 0.79 ng/g |
| 60 | Benzo(a)pyrene, per unit sediment mass | Benzo(a)pyrene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.35 ng/g, limit of quantification: 0.91 ng/g |
| 61 | Benzo(b)fluoranthene, per unit sediment mass | Benzo(b)fluoranthene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.31 ng/g, limit of quantification: 0.80 ng/g |
| 62 | Benzo(g,h,i)perylene, per unit sediment mass | Benzo(g,h,i)perylene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.05 ng/g, limit of quantification: 0.15 ng/g |
| 63 | Chrysene/Triphenylene, per unit sediment mass | Chrysene/Triphenylene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.08 ng/g, limit of quantification: 0.20 ng/g |
| 64 | Dibenz(a,h)anthracene, per unit sediment mass | Dibenz(ah)anthracene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.29 ng/g, limit of quantification: 0.75 ng/g |
| 65 | Fluoranthene, per unit sediment mass | Fluoranthene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.11 ng/g, limit of quantification: 0.30 ng/g |
| 66 | Fluorene, per unit sediment mass | Fluorene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.18 ng/g, limit of quantification: 0.47 ng/g |
| 67 | Indeno(1,2,3-cd)pyrene, per unit sediment mass | Indeno(1,2,3-cd)pyr/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.33 ng/g, limit of quantification: 0.86 ng/g |
| 68 | Naphthalene, per unit sediment mass | Naphth/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.26 ng/g, limit of quantification: 0.50 ng/g |
| 69 | Phenanthrene, per unit sediment mass | Phenanthrene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.10 ng/g, limit of quantification: 0.28 ng/g |
| 70 | Pyrene, per unit sediment mass | Pyrene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.21 ng/g, limit of quantification: 0.55 ng/g |
| 71 | 1-Methylnaphthalene, per unit sediment mass | 1-Methylnaphthalene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.10 ng/g, limit of quantification: 0.28 ng/g |
| 72 | 2-Methylnaphthalene, per unit sediment mass | 2-Methylnaphthalene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.17 ng/g, limit of quantification: 0.44 ng/g |
| 73 | 3-Methylphenanthrene, per unit sediment mass | 3-Methylphenanthrene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.45 ng/g, limit of quantification: 1.2 ng/g |
| 74 | 2,6-Dimethylnaphthalene, per unit sediment mass | 2,6-Dimethylnaphthalene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.07 ng/g, limit of quantification: 0.19 ng/g |
| 75 | 3,6-Dimethylphenanthrene, per unit sediment mass | 3,6-Dimethylphenanthrene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.29 ng/g, limit of quantification: 0.77 ng/g |
| 76 | 2,3,5-Trimethylnaphthalene, per unit sediment mass | 2,3,5-Trimethylnaphthalene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.04 ng/g, limit of quantification: 0.10 ng/g |
| 77 | 1,2,8-Trimethylphenanthrene, per unit sediment mass | 1,2,8-Trimethylphenanthrene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | measured in sediment, total, limit of detection: 0.09 ng/g, limit of quantification: 0.24 ng/g |
| 78 | Dimethylated Naphthalenes, per unit sediment mass | Dimethylated Naphthalene/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | sum, measured in sediment, total, limit of detection: 0.070 ng/g, limit of quantification: 0.19 ng/g |
| 79 | Trimethylated Naphthalenes, per unit sediment mass | Trimethylated Naphthalenes/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | sum, measured in sediment, total, limit of detection: 0.025 ng/g, limit of quantification: 0.64 ng/g |
| 80 | Methylated Phenantrenes, per unit sediment mass | Methylated Phenantrenes/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | sum, measured in sediment, total, limit of detection: 0.45 ng/g, limit of quantification: 1.2 ng/g |
| 81 | Dimethylated Phenantrenes, per unit sediment mass | Dimethylated Phenantrenes/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | sum, measured in sediment, total, limit of detection: 0.29 ng/g, limit of quantification: 0.76 ng/g |
| 82 | Trimethylated Phenantrenes, per unit sediment mass | Trimethylated Phenantrenes/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS/MS system (GC CP-3800, Varian) coupled to Varian 1200 (Varian) | sum, measured in sediment, total, limit of detection: 0.09 ng/g, limit of quantification: 0.24 ng/g |
| 83 | 2,4,4'-Trichlorobiphenyl, per unit sediment mass | 2,4,4-Trichlorobiphenyl/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, total, limit of detection: 0.004 ng/g, limit of quantification: 0.01 ng/g |
| 84 | 2,2',5,5'-Tetrachlorobiphenyl, per unit sediment mass | C12H6Cl4/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, total, limit of detection: 0.001 ng/g, limit of quantification: 0.002 ng/g |
| 85 | 2,2',4,5,5'-Pentachlorobiphenyl, per unit sediment mass | C12H5Cl5/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, total, limit of detection: 0.005 ng/g, limit of quantification: 0.01 ng/g |
| 86 | 2,3',4,4,5'-Pentachlorobiphenyl, per unit sediment mass | 2,3',4,4,5'-Pentachlorobiphenyl/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, total, limit of detection: 0.003 ng/g, limit of quantification: 0.007 ng/g |
| 87 | 2,2',3,4,4',5'-Hexachlorobiphenyl, per unit sediment mass | C12H4Cl6/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, total, limit of detection: 0.006 ng/g, limit of quantification: 0.01 ng/g |
| 88 | 2,2',4,4',5,5'-Hexachlorobiphenyl, per unit sediment mass | C12H4Cl6/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, total, limit of detection: 0.002 ng/g, limit of quantification: 0.005 ng/g |
| 89 | 2,2',3,4,4',5,5'-Heptachlorobiphenyl, per unit sediment mass | C12H3Cl7/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, total, limit of detection: 0.005 ng/g, limit of quantification: 0.01 ng/g |
| 90 | alpha-Hexachlorocyclohexane, per unit sediment mass | a-HCH/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, total, limit of detection: 0.01 ng/g, limit of quantification: 0.02 ng/g |
| 91 | beta-Hexachlorocyclohexane, per unit sediment mass | b-HCH/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, total, limit of detection: 0.005 ng/g, limit of quantification: 0.01 ng/g |
| 92 | gamma-Hexachlorocyclohexane, per unit sediment mass | g-HCH/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, total, limit of detection: 0.004 ng/g, limit of quantification: 0.01 ng/g |
| 93 | Hexachlorobenzene, per unit sediment mass | HCB/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, total, limit of detection: 0.002 ng/g, limit of quantification: 0.006 ng/g |
| 94 | para,para-Dichlorodiphenyldichloroethane, per unit sediment mass | pp-DDD/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, total, limit of detection: 0.007 ng/g, limit of quantification: 0.01 ng/g |
| 95 | para,para-Dichlorodiphenyldichloroethylene, per unit sediment mass | pp-DDE/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, total, limit of detection: 0.002 ng/g, limit of quantification: 0.005 ng/g |
| 96 | para,para-Dichlorodiphenyltrichloroethane, per unit sediment mass | pp-DDT/sed | ng/g | Logemann, Anna Elisabeth | Microwave extration, column clean-up, SEC, quantification via GC-MS ion-trap system (GC CP3800 coupled to a Saturn 2200, both Varian, CA, USA) | measured in sediment, total, limit of detection: 0.008 ng/g, limit of quantification: 0.01 ng/g |
License:
Creative Commons Attribution 4.0 International (CC-BY-4.0)
Status:
Curation Level: Enhanced curation (CurationLevelC)
Size:
1472 data points