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Fischer, Jonas; Talal, Ghanem; Schnee, Laura Sophie; Otomo, Patricks; Filser, Juliane (2022): Moulting test on the springtail Folsomia candida exposed via artificial test soils in a laboratory experiment [dataset]. PANGAEA, https://doi.org/10.1594/PANGAEA.949199, In: Fischer, J et al. (2022): Physiological, molecular and behavioural effects of copper oxide nanoparticles and copper chloride on the springtail Folsomia candida exposed via artificial test soils in a laboratory experiment [dataset bundled publication]. PANGAEA, https://doi.org/10.1594/PANGAEA.949202

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Abstract:
In a laboratory experiment, the soil invertebrate Folsomia candida (Collembola) was exposed to CuCl2 or copper oxide nanoparticles (CuO-NP) for 6 days. The animals were exposed via artificial test soil which varied in the size (19 or 30% of total mass) or the clay type of their clay fraction (kaolin or montmorillonite). The test substances were dissolved (CuCl2) or dispersed (CuO-NP) in pure miliQ water and stirred into the dry test soils to end up with test concentrations of 1, 3, 10 and 32 mg Cu/kg and a water content of 50% of the maximum water holding capacity of the respective soils. As a control, soil with miliQ water only was tested. For all soils, two tests with 5 replicates per treatment were conducted. At the beginning of the experiment, 30 animals at the age of 10-12 days were inserted into the test vessels containing the spiked test soil. After 6 days, all animals were extracted by floatation of the test soils with tap water and transferred to a Paris-plaster culture plate. After 2, 5 and 7 days, the exuviae shed by the animals were collected under a binocular and analysed for their total Cu content (not per biomass as mass of exuviae is too little to be measured) via atomic absorption spectroscopy (AAS). The number of shed exuviae per animal was calculated for each time point and statistically compared to the control by a linear mixed-effect model considering the two test runs as random factor. The Cu contents of the samples were analysed by an ordinal regression with respect to their ability to exceed the limit of detection or quantification in the AAS.
Keyword(s):
Artificial test soils; Catalase; copper; Copper oxide nanoparticles; Dry weight; Folsomia candida; Kaolin; Metallothionein; Montmorillonite; Moulting; Reproduction; Survival
Event(s):
Laboratory-experiments * Method/Device: Experiment (EXP)
Comment:
Funded by :
Hans‐Böckler‐Stiftung within the framework of the graduate school NanoCompetence (PK041). Open Access funding enabled and organized by Projekt DEAL.
Parameter(s):
#NameShort NameUnitPrincipal InvestigatorMethod/DeviceComment
ExperimentExpFischer, JonasTest name
Soil nameSoil nameFischer, JonasLaboratory experimentTest soil
TreatmentTreatFischer, JonasLaboratory experimentTreatment: test substance (NP, S) and the soil concentration of the respective Cu compound (1, 3, 10 or 32 mg Cu/kg), eg 3 mg Cu/kg with CuO-NP = NP-3; control (C).
Test substanceTest subsFischer, JonasLaboratory experimentTest substances: CuCl2 (S) and CuO-NP (NP), control (C) only contains miliQ water
Copper, per soil dry massCu soil dmmg/kgFischer, JonasLaboratory experiment
ReplicatesRepl#Fischer, JonasLaboratory experiment
Number of individualsInd No#Fischer, JonasLaboratory experimentUsed individuals
Time of dayTime of dayFischer, JonasLaboratory experimenta = 2 days, b = 5 days, d = 7 days
Folsomia candida, exuviaeF. candida exuviae#Fischer, JonasLaboratory experiment
10 Folsomia candida, exuviae, cumulatedF. candida exuviae cum#Fischer, JonasLaboratory experiment
11 Folsomia candida, exuviaeF. candida exuviae#Fischer, JonasLaboratory experimentper individual
12 Folsomia candida, exuviae, cumulatedF. candida exuviae cum#Fischer, JonasLaboratory experimentper individual
13 CopperCungFischer, JonasLaboratory experiment
14 Sample commentSample commentFischer, JonasLaboratory experimentData censoring criteria for Cu content
Status:
Curation Level: Enhanced curation (CurationLevelC)
Size:
6988 data points

Data

Download dataset as tab-delimited text — use the following character encoding:


Exp
(Test name)

Soil name
(Test soil)

Treat
(Treatment: test substance (NP...)

Test subs
(Test substances: CuCl2 (S) an...)

Cu soil dm [mg/kg]

Repl [#]

Ind No [#]
(Used individuals)

Time of day
(a = 2 days, b = 5 days, d = 7...)

F. candida exuviae [#]
10 
F. candida exuviae cum [#]
11 
F. candida exuviae [#]
(per individual)
12 
F. candida exuviae cum [#]
(per individual)
13 
Cu [ng]
14 
Sample comment
(Data censoring criteria for C...)
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Moulting-m30.2M30CC0522a550.2272727270.227272727
Moulting-m30.2M30CC0522b5100.2272727270.454545455
Moulting-m30.2M30CC0522d3130.1363636360.5909090910.376147711<LOD
Moulting-m30.2M30NP-1NP1124a880.3333333330.333333333
Moulting-m30.2M30NP-1NP1124b10180.4166666670.750000000
Moulting-m30.2M30NP-1NP1124d6240.2500000001.0000000000.678975634<LOQ
Moulting-m30.2M30NP-1NP1222a330.1363636360.136363636
Moulting-m30.2M30NP-1NP1222b470.1818181820.318181818
Moulting-m30.2M30NP-1NP1222d180.0454545450.3636363641.039094696<LOQ
Moulting-m30.2M30NP-1NP1323a440.1739130430.173913043
Moulting-m30.2M30NP-1NP1323b590.2173913040.391304348
Moulting-m30.2M30NP-1NP1323d7160.3043478260.6956521741.654168422>LOQ
Moulting-m30.2M30NP-1NP1423a440.1739130430.173913043
Moulting-m30.2M30NP-1NP1423b9130.3913043480.565217391
Moulting-m30.2M30NP-1NP1423d4170.1739130430.7391304352.892111842>LOQ
Moulting-m30.2M30NP-1NP1527a110.0370370370.037037037
Moulting-m30.2M30NP-1NP1527b18190.6666666670.703703704
Moulting-m30.2M30NP-1NP1527d6250.2222222220.9259259260.334985343<LOD
Moulting-m30.2M30NP-3NP3134a550.1470588240.147058824
Moulting-m30.2M30NP-3NP3134b6110.1764705880.323529412
Moulting-m30.2M30NP-3NP3134d5160.1470588240.4705882353.224426248>LOQ
Moulting-m30.2M30NP-3NP3212a220.1666666670.166666667
Moulting-m30.2M30NP-3NP3212b460.3333333330.500000000
Moulting-m30.2M30NP-3NP3212d280.1666666670.6666666670.637579762<LOQ
Moulting-m30.2M30NP-3NP3324a000.0000000000.000000000
Moulting-m30.2M30NP-3NP3324b13130.5416666670.541666667
Moulting-m30.2M30NP-3NP3324d4170.1666666670.7083333331.011306372<LOQ
Moulting-m30.2M30NP-3NP3424a660.2500000000.250000000
Moulting-m30.2M30NP-3NP3424b11170.4583333330.708333333
Moulting-m30.2M30NP-3NP3424d6230.2500000000.9583333330.472316286<LOD
Moulting-m30.2M30NP-3NP3522a110.0454545450.045454545
Moulting-m30.2M30NP-3NP3522b16170.7272727270.772727273
Moulting-m30.2M30NP-3NP3522d1180.0454545450.8181818180.582435148<LOQ
Moulting-m30.2M30NP-10NP10124a440.1666666670.166666667
Moulting-m30.2M30NP-10NP10124b480.1666666670.333333333
Moulting-m30.2M30NP-10NP10124d6140.2500000000.5833333330.458567346<LOD
Moulting-m30.2M30NP-10NP10213a660.4615384620.461538462
Moulting-m30.2M30NP-10NP10213b4100.3076923080.769230769
Moulting-m30.2M30NP-10NP10213d5150.3846153851.1538461542.748299124>LOQ
Moulting-m30.2M30NP-10NP1039a220.2222222220.222222222
Moulting-m30.2M30NP-10NP1039b570.5555555560.777777778
Moulting-m30.2M30NP-10NP1039d180.1111111110.8888888891.907881836>LOQ
Moulting-m30.2M30NP-10NP10412a000.0000000000.000000000
Moulting-m30.2M30NP-10NP10412b660.5000000000.500000000
Moulting-m30.2M30NP-10NP10412d4100.3333333330.8333333330.499824760<LOD
Moulting-m30.2M30NP-10NP10517a000.0000000000.000000000
Moulting-m30.2M30NP-10NP10517b660.3529411760.352941176
Moulting-m30.2M30NP-10NP10517d7130.4117647060.7647058820.252755145<LOD
Moulting-m30.2M30NP-32NP32130a770.2333333330.233333333
Moulting-m30.2M30NP-32NP32130b10170.3333333330.566666667
Moulting-m30.2M30NP-32NP32130d11280.3666666670.9333333330.472316286<LOD
Moulting-m30.2M30NP-32NP32217a660.3529411760.352941176
Moulting-m30.2M30NP-32NP32217b11170.6470588241.000000000
Moulting-m30.2M30NP-32NP32217d4210.2352941181.2352941180.637579762<LOD
Moulting-m30.2M30NP-32NP32315a440.2666666670.266666667
Moulting-m30.2M30NP-32NP32315b480.2666666670.533333333
Moulting-m30.2M30NP-32NP32315d5130.3333333330.8666666671.555833442>LOQ
Moulting-m30.2M30NP-32NP32420a550.2500000000.250000000
Moulting-m30.2M30NP-32NP32420b8130.4000000000.650000000
Moulting-m30.2M30NP-32NP32420d5180.2500000000.9000000000.803356456<LOD
Moulting-m30.2M30NP-32NP32516a110.0625000000.062500000
Moulting-m30.2M30NP-32NP32516b340.1875000000.250000000
Moulting-m30.2M30NP-32NP32516d590.3125000000.5625000000.568657883<LOD
Moulting-m30.2M30S-1S1130a110.0333333330.033333333
Moulting-m30.2M30S-1S1130b340.1000000000.133333333
Moulting-m30.2M30S-1S1130d9130.3000000000.4333333330.403606845<LOD
Moulting-m30.2M30S-1S1216a220.1250000000.125000000
Moulting-m30.2M30S-1S1216b350.1875000000.312500000
Moulting-m30.2M30S-1S1216d160.0625000000.3750000000.334985343<LOD
Moulting-m30.2M30S-1S1322a330.1363636360.136363636
Moulting-m30.2M30S-1S1322b7100.3181818180.454545455
Moulting-m30.2M30S-1S1322d5150.2272727270.6818181820.293854512<LOD
Moulting-m30.2M30S-1S1418a330.1666666670.166666667
Moulting-m30.2M30S-1S1418b580.2777777780.444444444
Moulting-m30.2M30S-1S1418d2100.1111111110.5555555560.789522012<LOQ
Moulting-m30.2M30S-1S1517a220.1176470590.117647059
Moulting-m30.2M30S-1S1517b460.2352941180.352941176
Moulting-m30.2M30S-1S1517d5110.2941176470.6470588240.886438760<LOQ
Moulting-m30.2M30S-3S3111a110.0909090910.090909091
Moulting-m30.2M30S-3S3111b450.3636363640.454545455
Moulting-m30.2M30S-3S3111d160.0909090910.5454545450.362423413<LOD
Moulting-m30.2M30S-3S3221a550.2380952380.238095238
Moulting-m30.2M30S-3S3221b9140.4285714290.666666667
Moulting-m30.2M30S-3S3221d3170.1428571430.8095238100.527347381<LOQ
Moulting-m30.2M30S-3S3310a000.0000000000.000000000
Moulting-m30.2M30S-3S3310b220.2000000000.200000000
Moulting-m30.2M30S-3S3310d460.4000000000.600000000
Moulting-m30.2M30S-3S3419a110.0526315790.052631579
Moulting-m30.2M30S-3S3419b890.4210526320.473684211
Moulting-m30.2M30S-3S3419d090.0000000000.4736842110.389875521<LOD
Moulting-m30.2M30S-3S3516a330.1875000000.187500000
Moulting-m30.2M30S-3S3516b7100.4375000000.625000000
Moulting-m30.2M30S-3S3516d0100.0000000000.6250000000.914161745<LOQ
Moulting-m30.2M30S-10S10122a110.0454545450.045454545
Moulting-m30.2M30S-10S10122b560.2272727270.272727273
Moulting-m30.2M30S-10S10122d9150.4090909090.6818181820.293854512<LOD
Moulting-m30.2M30S-10S10221a440.1904761900.190476190
Moulting-m30.2M30S-10S10221b12160.5714285710.761904762
Moulting-m30.2M30S-10S10221d1170.0476190480.8095238100.623788269<LOQ
Moulting-m30.2M30S-10S1033a000.0000000000.000000000
Moulting-m30.2M30S-10S1033b000.0000000000.000000000
Moulting-m30.2M30S-10S1033d110.3333333330.3333333330.928028667<LOQ
Moulting-m30.2M30S-10S10429a000.0000000000.000000000
Moulting-m30.2M30S-10S10429b440.1379310340.137931034
Moulting-m30.2M30S-10S10429d040.0000000000.1379310340.431080050<LOD
Moulting-m30.2M30S-10S10520a220.1000000000.100000000
Moulting-m30.2M30S-10S10520b350.1500000000.250000000
Moulting-m30.2M30S-10S10520d160.0500000000.3000000000.568657883<LOQ
Moulting-m30.2M30S-32S32120a000.0000000000.000000000
Moulting-m30.2M30S-32S32120b330.1500000000.150000000
Moulting-m30.2M30S-32S32120d470.2000000000.3500000000.403606845<LOD
Moulting-m30.2M30S-32S32220a000.0000000000.000000000
Moulting-m30.2M30S-32S32220b660.3000000000.300000000
Moulting-m30.2M30S-32S32220d390.1500000000.4500000000.156978577<LOD
Moulting-m30.2M30S-32S3237a000.0000000000.000000000
Moulting-m30.2M30S-32S3237b220.2857142860.285714286
Moulting-m30.2M30S-32S3237d350.4285714290.7142857143.036330218>LOQ
Moulting-m30.2M30S-32S32413a110.0769230770.076923077
Moulting-m30.2M30S-32S32413b450.3076923080.384615385
Moulting-m30.2M30S-32S32413d050.0000000000.3846153850.803356456<LOQ
Moulting-m30.2M30S-32S32516a000.0000000000.000000000
Moulting-m30.2M30S-32S32516b330.1875000000.187500000
Moulting-m30.2M30S-32S32516d8110.5000000000.6875000000.389875521<LOD
Moulting-k30.2K30CC0119a770.3684210530.368421053
Moulting-k30.2K30CC0119b14210.7368421051.105263158
Moulting-k30.2K30CC0119d10310.5263157891.6315789470.839387686<LOQ
Moulting-k30.2K30CC0223a15150.6521739130.652173913
Moulting-k30.2K30CC0223b13280.5652173911.217391304
Moulting-k30.2K30CC0223d10380.4347826091.6521739131.199632211<LOQ
Moulting-k30.2K30CC0324a990.3750000000.375000000
Moulting-k30.2K30CC0324b16250.6666666671.041666667
Moulting-k30.2K30CC0324d7320.2916666671.3333333331.113355153<LOQ
Moulting-k30.2K30CC0420a440.2000000000.200000000
Moulting-k30.2K30CC0420b15190.7500000000.950000000
Moulting-k30.2K30CC0420d10290.5000000001.4500000000.723686298<LOQ
Moulting-k30.2K30CC0525a15150.6000000000.600000000
Moulting-k30.2K30CC0525b14290.5600000001.160000000
Moulting-k30.2K30CC0525d4330.1600000001.3200000000.810481689<LOQ
Moulting-k30.2K30NP-1NP1122a11110.5000000000.500000000
Moulting-k30.2K30NP-1NP1122b19300.8636363641.363636364
Moulting-k30.2K30NP-1NP1122d7370.3181818181.6818181820.694728645<LOQ
Moulting-k30.2K30NP-1NP1214a770.5000000000.500000000
Moulting-k30.2K30NP-1NP1214b12190.8571428571.357142857
Moulting-k30.2K30NP-1NP1214d6250.4285714291.7857142860.824936297<LOQ
Moulting-k30.2K30NP-1NP1324a880.3333333330.333333333
Moulting-k30.2K30NP-1NP1324b14220.5833333330.916666667
Moulting-k30.2K30NP-1NP1324d8300.3333333331.2500000003.097608782<LOD
Moulting-k30.2K30NP-1NP1414a12120.8571428570.857142857
Moulting-k30.2K30NP-1NP1414b11230.7857142861.642857143
Moulting-k30.2K30NP-1NP1414d4270.2857142861.9285714293.750732371<LOD
Moulting-k30.2K30NP-1NP1526a220.0769230770.076923077
Moulting-k30.2K30NP-1NP1526b16180.6153846150.692307692
Moulting-k30.2K30NP-1NP1526d13310.5000000001.1923076921.041370249<LOQ
Moulting-k30.2K30NP-3NP3117a550.2941176470.294117647
Moulting-k30.2K30NP-3NP3117b9140.5294117650.823529412
Moulting-k30.2K30NP-3NP3117d6200.3529411761.1764705880.709209090<LOQ
Moulting-k30.2K30NP-3NP3222a330.1363636360.136363636
Moulting-k30.2K30NP-3NP3222b9120.4090909090.545454545
Moulting-k30.2K30NP-3NP3222d9210.4090909090.9545454550.723686298<LOQ
Moulting-k30.2K30NP-3NP3323a330.1304347830.130434783
Moulting-k30.2K30NP-3NP3323b15180.6521739130.782608696
Moulting-k30.2K30NP-3NP3323d6240.2608695651.0434782610.506187285<LOD
Moulting-k30.2K30NP-3NP3422a440.1818181820.181818182
Moulting-k30.2K30NP-3NP3422b14180.6363636360.818181818
Moulting-k30.2K30NP-3NP3422d3210.1363636360.9545454550.389887646<LOD
Moulting-k30.2K30NP-3NP3529a440.1379310340.137931034
Moulting-k30.2K30NP-3NP3529b10140.3448275860.482758621
Moulting-k30.2K30NP-3NP3529d7210.2413793100.7241379310.796023858<LOQ
Moulting-k30.2K30NP-10NP10120a880.4000000000.400000000
Moulting-k30.2K30NP-10NP10120b12200.6000000001.000000000
Moulting-k30.2K30NP-10NP10120d2220.1000000001.1000000000.824936297<LOQ
Moulting-k30.2K30NP-10NP10222a440.1818181820.181818182
Moulting-k30.2K30NP-10NP10222b11150.5000000000.681818182
Moulting-k30.2K30NP-10NP10222d8230.3636363641.0454545450.389887646<LOD
Moulting-k30.2K30NP-10NP10322a550.2272727270.227272727
Moulting-k30.2K30NP-10NP10322b10150.4545454550.681818182
Moulting-k30.2K30NP-10NP10322d8230.3636363641.0454545451.386175597<LOQ
Moulting-k30.2K30NP-10NP10422a880.3636363640.363636364
Moulting-k30.2K30NP-10NP10422b12200.5454545450.909090909
Moulting-k30.2K30NP-10NP10422d2220.0909090911.0000000000.796023858<LOQ
Moulting-k30.2K30NP-10NP10519a220.1052631580.105263158
Moulting-k30.2K30NP-10NP10519b350.1578947370.263157895
Moulting-k30.2K30NP-10NP10519d6110.3157894740.5789473682.141258114>LOQ
Moulting-k30.2K30NP-32NP32120a440.2000000000.200000000
Moulting-k30.2K30NP-32NP32120b12160.6000000000.800000000
Moulting-k30.2K30NP-32NP32120d6220.3000000001.1000000000.448063679<LOD
Moulting-k30.2K30NP-32NP32222a220.0909090910.090909091
Moulting-k30.2K30NP-32NP32222b14160.6363636360.727272727
Moulting-k30.2K30NP-32NP32222d5210.2272727270.9545454554.780116832>LOQ
Moulting-k30.2K30NP-32NP32315a770.4666666670.466666667
Moulting-k30.2K30NP-32NP32315b9160.6000000001.066666667
Moulting-k30.2K30NP-32NP32315d6220.4000000001.4666666671.257086928<LOQ
Moulting-k30.2K30NP-32NP32410a330.3000000000.300000000
Moulting-k30.2K30NP-32NP32410b7100.7000000001.000000000
Moulting-k30.2K30NP-32NP32410d1110.1000000001.1000000000.317093665<LOQ
Moulting-k30.2K30NP-32NP32521a550.2380952380.238095238
Moulting-k30.2K30NP-32NP32521b7120.3333333330.571428571
Moulting-k30.2K30NP-32NP32521d7190.3333333330.9047619050.651267864<LOQ
Moulting-k30.2K30S-1S1115a990.6000000000.600000000
Moulting-k30.2K30S-1S1115b2110.1333333330.733333333
Moulting-k30.2K30S-1S1115d7180.4666666671.2000000000.593274705<LOD
Moulting-k30.2K30S-1S1219a550.2631578950.263157895
Moulting-k30.2K30S-1S1219b12170.6315789470.894736842
Moulting-k30.2K30S-1S1219d5220.2631578951.1578947370.549745670<LOD
Moulting-k30.2K30S-1S1316a440.2500000000.250000000
Moulting-k30.2K30S-1S1316b590.3125000000.562500000
Moulting-k30.2K30S-1S1316d7160.4375000001.0000000001.084570738<LOQ
Moulting-k30.2K30S-1S146a110.1666666670.166666667
Moulting-k30.2K30S-1S146b230.3333333330.500000000
Moulting-k30.2K30S-1S146d250.3333333330.8333333331.285795340<LOQ
Moulting-k30.2K30S-1S1515a990.6000000000.600000000
Moulting-k30.2K30S-1S1515b7160.4666666671.066666667
Moulting-k30.2K30S-1S1515d8240.5333333331.6000000000.389887646<LOD
Moulting-k30.2K30S-3S3118a11110.6111111110.611111111
Moulting-k30.2K30S-3S3118b7180.3888888891.000000000
Moulting-k30.2K30S-3S3118d8260.4444444441.4444444440.520710012<LOD
Moulting-k30.2K30S-3S3228a880.2857142860.285714286
Moulting-k30.2K30S-3S3228b6140.2142857140.500000000
Moulting-k30.2K30S-3S3228d7210.2500000000.7500000000.215043570<LOD
Moulting-k30.2K30S-3S3320a660.3000000000.300000000
Moulting-k30.2K30S-3S3320b15210.7500000001.050000000
Moulting-k30.2K30S-3S3320d4250.2000000001.2500000000.868280813<LOQ
Moulting-k30.2K30S-3S3418a110.0555555560.055555556
Moulting-k30.2K30S-3S3418b10110.5555555560.611111111
Moulting-k30.2K30S-3S3418d4150.2222222220.8333333330.491661290<LOD
Moulting-k30.2K30S-3S3512a000.0000000000.000000000
Moulting-k30.2K30S-3S3512b990.7500000000.750000000
Moulting-k30.2K30S-3S3512d5140.4166666671.1666666670.651267864<LOQ
Moulting-k30.2K30S-10S10118a770.3888888890.388888889
Moulting-k30.2K30S-10S10118b16230.8888888891.277777778
Moulting-k30.2K30S-10S10118d4270.2222222221.5000000000.578768284<LOD
Moulting-k30.2K30S-10S10219a330.1578947370.157894737
Moulting-k30.2K30S-10S10219b360.1578947370.315789474
Moulting-k30.2K30S-10S10219d12180.6315789470.9473684210.853835858<LOQ
Moulting-k30.2K30S-10S10319a440.2105263160.210526316
Moulting-k30.2K30S-10S10319b15190.7894736841.000000000
Moulting-k30.2K30S-10S10319d2210.1052631581.1052631580.302524988<LOD
Moulting-k30.2K30S-10S10416a440.2500000000.250000000
Moulting-k30.2K30S-10S10416b9130.5625000000.812500000
Moulting-k30.2K30S-10S10416d3160.1875000001.0000000000.258799154<LOD
Moulting-k30.2K30S-10S1055a000.0000000000.000000000
Moulting-k30.2K30S-10S1055b330.6000000000.600000000
Moulting-k30.2K30S-10S1055d030.0000000000.6000000000.215043570<LOD
Moulting-k30.2K30S-32S32116a220.1250000000.125000000
Moulting-k30.2K30S-32S32116b10120.6250000000.750000000
Moulting-k30.2K30S-32S32116d3150.1875000000.9375000000.462599489<LOD
Moulting-k30.2K30S-32S32215a550.3333333330.333333333
Moulting-k30.2K30S-32S32215b12170.8000000001.133333333
Moulting-k30.2K30S-32S32215d2190.1333333331.2666666670.331659046<LOD
Moulting-k30.2K30S-32S32317a440.2352941180.235294118
Moulting-k30.2K30S-32S32317b6100.3529411760.588235294
Moulting-k30.2K30S-32S32317d6160.3529411760.9411764710.564258607<LOD
Moulting-k30.2K30S-32S32412a880.6666666670.666666667
Moulting-k30.2K30S-32S32412b5130.4166666671.083333333
Moulting-k30.2K30S-32S32412d3160.2500000001.3333333331.142126859<LOQ
Moulting-k30.2K30S-32S3259a110.1111111110.111111111
Moulting-k30.2K30S-32S3259b340.3333333330.444444444
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Moulting-k30.3K30S-10S10417d680.3529411760.4705882353.212277433>LOQ
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Moulting-k30.3K30S-32S32314d580.3571428570.5714285714.830913142>LOQ
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