Martinez, Andres; Hua, Jason; Haque, Ezazul; Thorne, Peter; Hornbuckle, Keri C (2022): Concentrations of individual polychlorinated biphenyl congeners from Standard Reference Material (SRM) 1944 [dataset]. PANGAEA, https://doi.org/10.1594/PANGAEA.941883, In: Martinez, A et al. (2022): Dataset of concentrations of individual polychlorinated biphenyl congeners and total organic carbon in soils from East Chicago, Indiana, USA in 2017/2018 [dataset bundled publication]. PANGAEA, https://doi.org/10.1594/PANGAEA.941894
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Abstract:
Five Standard Reference Material 1944, New York, New Jersey Waterway sediment (SRM 1944, National Institutes of Standards and Testing) were extracted, cleaned and quantified using the same method for soils. Gas chromatography (GC) in tandem with Mass Spectrometry GC-MS/MS (Agilent 7000) in multiple reaction monitoring (MRM) mode was used to quantify all 28 individual or coeluting certified congeners. The GC was equipped with a Supelco SBP-Octyl capillary column (30 m × 0.25 mm ID, 0.25 mm film thicknesses) with helium as carrier gas.
Supplement to:
Martinez, Andres; Hua, Jason; Haque, Ezazul; Hornbuckle, Keri C; Thorne, Peter (2022): Occurrence and spatial distribution of individual polychlorinated biphenyl congeners in residential soils from East Chicago, southwest Lake Michigan. Science of the Total Environment, 850, 157705, https://doi.org/10.1016/j.scitotenv.2022.157705
Funding:
National Institute of Environmental Health Sciences (NIEHS), grant/award no. P42ES013661: Iowa Superfund Research Program
National Institutes of Health (NIH), grant/award no. P30ES005605: University of Iowa's Environmental Health Sciences Research Center
Comment:
Selected PCB congener in sediment Standard Reference Material (R) 1944 using GC-MS/MS:
* The congeners with an asterisk indicate the main congener identified by the reference material.
* Our analytical method yields a different congener separation.
Parameter(s):
| # | Name | Short Name | Unit | Principal Investigator | Method/Device | Comment |
|---|---|---|---|---|---|---|
| 1 | Sample code/label | Sample label | Martinez, Andres | |||
| 2 | Method comment | Method comm | Martinez, Andres | |||
| 3 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB8 |
| 4 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB18*+30 |
| 5 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB20+28* |
| 6 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB31 |
| 7 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB44*+47+65 |
| 8 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB49*+69 |
| 9 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB52 |
| 10 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB66 |
| 11 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB87*+125 |
| 12 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB95 |
| 13 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB99 |
| 14 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB90+101*+113 |
| 15 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB105 |
| 16 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB110 |
| 17 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB118 |
| 18 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB129+138*+163 |
| 19 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB147+149* |
| 20 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB135+151* |
| 21 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB153*+168 |
| 22 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB156*+157 |
| 23 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB170 |
| 24 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB180*+193 |
| 25 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB183 |
| 26 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB187 |
| 27 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB194 |
| 28 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB195 |
| 29 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB206 |
| 30 | Polychlorinated biphenyl, per unit sediment dry mass | PCB/sed dm | ng/g | Martinez, Andres | tandem mass spectrometry (GC-MS/MS) in multiple reaction monitoring mode (MRM) | PCB209 |
License:
Creative Commons Attribution 4.0 International (CC-BY-4.0)
Status:
Curation Level: Enhanced curation (CurationLevelC)
Size:
150 data points
Data
| 1 Sample label | 2 Method comm | 3 PCB/sed dm [ng/g] (PCB8) | 4 PCB/sed dm [ng/g] (PCB18*+30) | 5 PCB/sed dm [ng/g] (PCB20+28*) | 6 PCB/sed dm [ng/g] (PCB31) | 7 PCB/sed dm [ng/g] (PCB44*+47+65) | 8 PCB/sed dm [ng/g] (PCB49*+69) | 9 PCB/sed dm [ng/g] (PCB52) | 10 PCB/sed dm [ng/g] (PCB66) | 11 PCB/sed dm [ng/g] (PCB87*+125) | 12 PCB/sed dm [ng/g] (PCB95) | 13 PCB/sed dm [ng/g] (PCB99) | 14 PCB/sed dm [ng/g] (PCB90+101*+113) | 15 PCB/sed dm [ng/g] (PCB105) | 16 PCB/sed dm [ng/g] (PCB110) | 17 PCB/sed dm [ng/g] (PCB118) | 18 PCB/sed dm [ng/g] (PCB129+138*+163) | 19 PCB/sed dm [ng/g] (PCB147+149*) | 20 PCB/sed dm [ng/g] (PCB135+151*) | 21 PCB/sed dm [ng/g] (PCB153*+168) | 22 PCB/sed dm [ng/g] (PCB156*+157) | 23 PCB/sed dm [ng/g] (PCB170) | 24 PCB/sed dm [ng/g] (PCB180*+193) | 25 PCB/sed dm [ng/g] (PCB183) | 26 PCB/sed dm [ng/g] (PCB187) | 27 PCB/sed dm [ng/g] (PCB194) | 28 PCB/sed dm [ng/g] (PCB195) | 29 PCB/sed dm [ng/g] (PCB206) | 30 PCB/sed dm [ng/g] (PCB209) |
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| SRM1 | individual PCB congener in SRM ng per g d.w. | 17.28479 | 38.89699 | 87.57892 | 68.31723 | 59.49361 | 40.33336 | 75.26084 | 45.96602 | 19.15466 | 37.22681 | 25.20598 | 57.05868 | 23.65921 | 60.03437 | 50.67906 | 49.13272 | 14.06971 | 37.46780 | 42.10081 | 5.05065 | 12.97190 | 29.05678 | 8.82479 | 16.84086 | 6.98289 | 2.52658 | 5.27403 | 4.42509 |
| SRM2 | individual PCB congener in SRM ng per g d.w. | 18.33150 | 39.63911 | 90.51221 | 70.01905 | 62.91650 | 42.54118 | 80.14138 | 49.87848 | 20.70758 | 39.93390 | 26.78320 | 61.18221 | 25.09590 | 63.85473 | 54.11910 | 52.79265 | 14.95041 | 38.99984 | 44.22216 | 5.28956 | 13.73937 | 30.17459 | 8.11506 | 17.61112 | 7.88559 | 2.88636 | 5.82697 | 4.70280 |
| SRM3 | individual PCB congener in SRM ng per g d.w. | 17.45338 | 38.28731 | 87.14823 | 69.46840 | 61.81554 | 42.26305 | 78.43184 | 46.01580 | 20.02031 | 38.94587 | 25.72449 | 60.21389 | 25.12240 | 62.95584 | 53.48834 | 49.62048 | 14.84808 | 38.63914 | 42.50257 | 5.34634 | 13.59823 | 29.68678 | 8.04449 | 17.12001 | 7.70064 | 2.92296 | 5.62585 | 4.61027 |
| SRM4 | individual PCB congener in SRM ng per g d.w. | 17.87743 | 39.66337 | 89.86832 | 69.57278 | 61.84425 | 41.72020 | 77.10223 | 46.82915 | 20.12370 | 37.59557 | 24.97434 | 58.99156 | 24.92329 | 61.01181 | 52.28237 | 52.31964 | 14.81436 | 38.51013 | 44.66182 | 5.25570 | 19.74501 | 47.82117 | 12.54715 | 25.31449 | 16.74496 | 6.32726 | 8.49200 | 4.87154 |
| SRM5 | individual PCB congener in SRM ng per g d.w. | 17.88410 | 40.00648 | 89.75065 | 67.70897 | 62.07723 | 42.37680 | 77.18262 | 44.60475 | 20.25618 | 38.16686 | 24.89366 | 58.46173 | 24.55348 | 60.64439 | 51.36433 | 51.04737 | 14.51318 | 37.78902 | 42.17219 | 5.25948 | 14.24351 | 30.18511 | 7.35439 | 17.94202 | 7.41360 | 2.95027 | 5.54449 | 4.74295 |