Citation:

PANGAEA.918317

Name: Polar lipid-derived fatty acids (PLFAs) of surface samples from the Wadden Sea
Published: 2020-06-04
License: https://creativecommons.org/licenses/by/4.0/
Keywords: bacterial community functions; metabolic pathways; polar lipid-derived fatty acids; position-specific labeling; stable isotope probing; substrate specificity

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Keyword(s):

bacterial community functions; metabolic pathways; polar lipid-derived fatty acids; position-specific labeling; stable isotope probing; substrate specificity

Related to:

Aepfler, Rebecca F; Bühring, Solveig I; Elvert, Marcus (2019): Substrate characteristic bacterial fatty acid production based on amino acid assimilation and transformation in marine sediments. FEMS Microbiology Ecology, 95(10), https://doi.org/10.1093/femsec/fiz131

Project(s):

Center for Marine Environmental Sciences (MARUM)

Coverage:

Latitude: 53.733333 * Longitude: 8.500000

Minimum DEPTH, sediment/rock: 0.02 m * Maximum DEPTH, sediment/rock: 0.02 m

Event(s):

Wadden_Sea_surface * Latitude: 53.733333 * Longitude: 8.500000 * Location: Wadden Sea, Germany

Comment:

* C15:1-I and C15:1-II are tentatively assigned as C15:1ω8 and C15:1ω6 (molecule structures were not identifiable entirely in terms of their double bound-positions).

** iC17:1-I and iC17:1-II can be assumed to embody the fatty acids iC17:1ω8 and iC17:1ω6 (molecule structures were not identifiable entirely in terms of their double bound-positions).

*** has not been separated from following peaks distinctly enough for accurate isotopic value determination.

Duplicate measurements of the incubated samples held deviations of the FA concentrations of ±4.7 ng PLFA g−1 (C13:0 with a concentration of 33.2 ng PLFA g−1) to ±877 ng PLFA g−1 (C16:0 with a concentration of 11 500 ng PLFA g−1). Deviations of the δ13C values were between <0.1 and ±69.4‰ (for PLFAs with label uptake of >700‰).

Parameter(s):

#	Name	Short Name	Unit	Principal Investigator	Comment
1	DEPTH, sediment/rock	Depth sed	m	Aepfler, Rebecca F	Geocode
2	Depth, top/min	Depth top	m	Aepfler, Rebecca F
3	Depth, bottom/max	Depth bot	m	Aepfler, Rebecca F
4	Experiment	Exp		Aepfler, Rebecca F
5	Time in hours	Time	h	Aepfler, Rebecca F
6	Comment	Comment		Aepfler, Rebecca F
7	iso-fatty acid C13:0	i-C13:0	ng/g	Aepfler, Rebecca F
8	n-fatty acid C13:0	n-C13:0	ng/g	Aepfler, Rebecca F
9	iso-fatty acid C14:0	i-C14:0	ng/g	Aepfler, Rebecca F
10	n-fatty acid C14:1w7	n-C14:1w7	ng/g	Aepfler, Rebecca F
11	n-fatty acid C14:0	n-C14:0	ng/g	Aepfler, Rebecca F
12	iso-fatty acid C15:0	i-C15:0	ng/g	Aepfler, Rebecca F
13	anteiso-fatty acid aiC15:0	ai-C15:0	ng/g	Aepfler, Rebecca F
14	n-fatty acid C15:1-I	n-C15:1-I	ng/g	Aepfler, Rebecca F	*
15	n-fatty acid C15:1-II	n-C15:1-II	ng/g	Aepfler, Rebecca F	*
16	n-fatty acid C15:0	n-C15:0	ng/g	Aepfler, Rebecca F
17	iso-fatty acid C16:0	i-C16:0	ng/g	Aepfler, Rebecca F
18	n-fatty acid C16:3	n-C16:3	ng/g	Aepfler, Rebecca F
19	n-fatty acid C16:1w7cis/trans	n-C16:1w7c/t	ng/g	Aepfler, Rebecca F
20	n-fatty acid C16:1w5	n-C16:1w5	ng/g	Aepfler, Rebecca F
21	n-fatty acid C16:0	n-C16:0	ng/g	Aepfler, Rebecca F
22	iso-fatty acid C17:1-I	i-C17:1-I	ng/g	Aepfler, Rebecca F	**
23	iso-fatty acid C17:1-II	i-C17:1-II	ng/g	Aepfler, Rebecca F	**
24	10Me-C16:0	10Me-C16:0	ng/g	Aepfler, Rebecca F
25	iso-fatty acid C17:0	i-C17:0	ng/g	Aepfler, Rebecca F
26	anteiso-fatty acid aiC17:0	ai-C17:0	ng/g	Aepfler, Rebecca F	***
27	n-fatty acid C17:1w8	n-C17:1w8	ng/g	Aepfler, Rebecca F
28	n-fatty acid C17:1w6	n-C17:1w6	ng/g	Aepfler, Rebecca F
29	n-fatty acid C17:0	n-C17:0	ng/g	Aepfler, Rebecca F
30	n-fatty acid C18:3	n-C18:3	ng/g	Aepfler, Rebecca F
31	n-fatty acid C18:4	n-C18:4	ng/g	Aepfler, Rebecca F
32	n-fatty acid C18:2	n-C18:2	ng/g	Aepfler, Rebecca F
33	n-fatty acid C18:1w9	n-C18:1w9	ng/g	Aepfler, Rebecca F
34	n-fatty acid C18:1w7cis	n-C18:1w7c	ng/g	Aepfler, Rebecca F
35	n-fatty acid C18:1w7trans	n-C18:1w7t	ng/g	Aepfler, Rebecca F
36	n-fatty acid C18:0	n-C18:0	ng/g	Aepfler, Rebecca F
37	n-fatty acid C20:4	n-C20:4	ng/g	Aepfler, Rebecca F
38	n-fatty acid C20:5	n-C20:5	ng/g	Aepfler, Rebecca F
39	iso-fatty acid C13:0, δ13C	i-C13:0 δ13C	‰ PDB	Aepfler, Rebecca F
40	n-fatty acid C13:0, δ13C	n-C13:0 δ13C	‰ PDB	Aepfler, Rebecca F
41	iso-fatty acid C14:0, δ13C	i-C14:0 δ13C	‰ PDB	Aepfler, Rebecca F
42	n-fatty acid C14:1w7, δ13C	n-C14:1w7 δ13C	‰ PDB	Aepfler, Rebecca F
43	n-fatty acid C14:0, δ13C	n-C14:0 δ13C	‰ PDB	Aepfler, Rebecca F
44	iso-fatty acid C15:0, δ13C	i-C15:0 δ13C	‰ PDB	Aepfler, Rebecca F
45	anteiso-fatty acid C15:0, δ13C	ai-C15:0 δ13C	‰ PDB	Aepfler, Rebecca F
46	n-fatty acid C15:1-I, δ13C	n-C15:1-I δ13C	‰ PDB	Aepfler, Rebecca F	*
47	n-fatty acid C15:1-II, δ13C	n-C15:1-II δ13C	‰ PDB	Aepfler, Rebecca F	*
48	n-fatty acid C15:0, δ13C	n-C15:0 δ13C	‰ PDB	Aepfler, Rebecca F
49	iso-fatty acid C16:0, δ13C	i-C16:0 δ13C	‰ PDB	Aepfler, Rebecca F
50	n-fatty acid C16:3, δ13C	n-C16:3 δ13C	‰ PDB	Aepfler, Rebecca F
51	n-fatty acid C16:1w7cis/trans, δ13C	n-C16:1w7c/t δ13C	‰ PDB	Aepfler, Rebecca F
52	n-fatty acid C16:1w5, δ13C	n-C16:1w5 δ13C	‰ PDB	Aepfler, Rebecca F
53	n-fatty acid C16:0, δ13C	n-C16:0 δ13C	‰ PDB	Aepfler, Rebecca F
54	iso-fatty acid C17:1-I, δ13C	i-C17:1-I δ13C	‰ PDB	Aepfler, Rebecca F	**
55	iso-fatty acid C17:1-II, δ13C	i-C17:1-II δ13C	‰ PDB	Aepfler, Rebecca F	**
56	10Me-C16:0, δ13C	10Me-C16:0 δ13C	‰ PDB	Aepfler, Rebecca F
57	iso-fatty acid C17:0, δ13C	i-C17:0 δ13C	‰ PDB	Aepfler, Rebecca F
58	anteiso-fatty acid C17:0, δ13C	ai-C17:0 δ13C	‰ PDB	Aepfler, Rebecca F	***
59	n-fatty acid C17:1w8, δ13C	n-C17:1w8 δ13C	‰ PDB	Aepfler, Rebecca F
60	n-fatty acid C17:1w6, δ13C	n-C17:1w6 δ13C	‰ PDB	Aepfler, Rebecca F
61	n-fatty acid C17:0, δ13C	n-C17:0 δ13C	‰ PDB	Aepfler, Rebecca F
62	n-fatty acid C18:3, δ13C	n-C18:3 δ13C	‰ PDB	Aepfler, Rebecca F
63	n-fatty acid C18:4, δ13C	n-C18:4 δ13C	‰ PDB	Aepfler, Rebecca F
64	n-fatty acid C18:2, δ13C	n-C18:2 δ13C	‰ PDB	Aepfler, Rebecca F
65	n-fatty acid C18:1w9, δ13C	n-C18:1w9 δ13C	‰ PDB	Aepfler, Rebecca F
66	n-fatty acid C18:1w7cis, δ13C	n-C18:1w7c δ13C	‰ PDB	Aepfler, Rebecca F
67	n-fatty acid C18:1w7trans, δ13C	n-C18:1w7t δ13C	‰ PDB	Aepfler, Rebecca F
68	n-fatty acid C18:0, δ13C	n-C18:0 δ13C	‰ PDB	Aepfler, Rebecca F
69	n-fatty acid C20:4, δ13C	n-C20:4 δ13C	‰ PDB	Aepfler, Rebecca F
70	n-fatty acid C20:5, δ13C	n-C20:5 δ13C	‰ PDB	Aepfler, Rebecca F

License:

Creative Commons Attribution 4.0 International (CC-BY-4.0)

Size:

1608 data points

Data

Download dataset as tab-delimited text — use the following character encoding:

1 Depth sed [m]	2 Depth top [m]	3 Depth bot [m]	4 Exp	5 Time [h]	6 Comment	7 i-C13:0 [ng/g]	8 n-C13:0 [ng/g]	9 i-C14:0 [ng/g]	10 n-C14:1w7 [ng/g]	11 n-C14:0 [ng/g]	12 i-C15:0 [ng/g]	13 ai-C15:0 [ng/g]	14 n-C15:1-I [ng/g]	15 n-C15:1-II [ng/g]	16 n-C15:0 [ng/g]	17 i-C16:0 [ng/g]	18 n-C16:3 [ng/g]	19 n-C16:1w7c/t [ng/g]	20 n-C16:1w5 [ng/g]	21 n-C16:0 [ng/g]	22 i-C17:1-I [ng/g]	23 i-C17:1-II [ng/g]	24 10Me-C16:0 [ng/g]	25 i-C17:0 [ng/g]	26 ai-C17:0 [ng/g]	27 n-C17:1w8 [ng/g]	28 n-C17:1w6 [ng/g]	29 n-C17:0 [ng/g]	30 n-C18:3 [ng/g]	31 n-C18:4 [ng/g]	32 n-C18:2 [ng/g]	33 n-C18:1w9 [ng/g]	34 n-C18:1w7c [ng/g]	35 n-C18:1w7t [ng/g]	36 n-C18:0 [ng/g]	37 n-C20:4 [ng/g]	38 n-C20:5 [ng/g]	39 i-C13:0 δ13C [‰ PDB]	40 n-C13:0 δ13C [‰ PDB]	41 i-C14:0 δ13C [‰ PDB]	42 n-C14:1w7 δ13C [‰ PDB]	43 n-C14:0 δ13C [‰ PDB]	44 i-C15:0 δ13C [‰ PDB]	45 ai-C15:0 δ13C [‰ PDB]	46 n-C15:1-I δ13C [‰ PDB]	47 n-C15:1-II δ13C [‰ PDB]	48 n-C15:0 δ13C [‰ PDB]	49 i-C16:0 δ13C [‰ PDB]	50 n-C16:3 δ13C [‰ PDB]	51 n-C16:1w7c/t δ13C [‰ PDB]	52 n-C16:1w5 δ13C [‰ PDB]	53 n-C16:0 δ13C [‰ PDB]	54 i-C17:1-I δ13C [‰ PDB]	55 i-C17:1-II δ13C [‰ PDB]	56 10Me-C16:0 δ13C [‰ PDB]	57 i-C17:0 δ13C [‰ PDB]	58 ai-C17:0 δ13C [‰ PDB]	59 n-C17:1w8 δ13C [‰ PDB]	60 n-C17:1w6 δ13C [‰ PDB]	61 n-C17:0 δ13C [‰ PDB]	62 n-C18:3 δ13C [‰ PDB]	63 n-C18:4 δ13C [‰ PDB]	64 n-C18:2 δ13C [‰ PDB]	65 n-C18:1w9 δ13C [‰ PDB]	66 n-C18:1w7c δ13C [‰ PDB]	67 n-C18:1w7t δ13C [‰ PDB]	68 n-C18:0 δ13C [‰ PDB]	69 n-C20:4 δ13C [‰ PDB]	70 n-C20:5 δ13C [‰ PDB]
0.02	0.01	0.03	Alanine-3-13C-Experiment		Background		102.0	119.0	63.3	915	385	432	81.7	270	1020	370		8370	656	5340	50.6	47.5	235	74.0	28.8	667	149	268			248	656	606	56.8	631	1160	1090		-22.9	-22.3	-15.0	-18.1	-19.9	-18.6	-21.9	-17.6	-18.5	-18.8		-15.1	-37.6	-19.1	-9.7	-18.1	-27.5	-24.9	-19.8	-18.7	-26.6	-20.5			-22.9	-19.5	-22.3	-35.3	-21.4	-16.6	-18.8
0.02	0.01	0.03	Alanine-3-13C-Experiment	0			57.0	113.0	39.4	1040	496	530	92.2	244	1340	315		10100	201	7370	25.9	49.8	123	74.0	62.5	821	270	444			261	875	1320	56.6	803	2600	2970		-16.7	-19.1	-14.5	-18.8	-19.2	-18.8	-21.8	-18.4	-18.3	-10.6		-14.8	-34.6	-18.9	-4.8	-17.1	-27.7	-18.1	-3.9	-19.4	-28.5	-19.0			-17.2	-19.3	-20.4	-35.7	-22.4	-18.3	-22.4
0.02	0.01	0.03	Alanine-3-13C-Experiment	3			94.8	120.0	56.7	953	450	491	85.8	246	1070	398		8820	591	5390	22.8	51.1	117	41.4	34.4	643	192	311			199	712	771	57.8	635	1560	1560		-12.6	-3.4	4.4	-11.7	39.6	8.8	-10.7	6.7	-12.2	-4.3		-14.0	-27.1	-13.5	-2.9	32.6	-12.5	16.7	13.7	-10.3	6.0	-9.4			-15.7	-17.7	-10.1	-11.6	-15.0	-20.4	-19.9
0.02	0.01	0.03	Alanine-3-13C-Experiment	6			54.4	103.0	36.7	905	461	478	75.3	217	1180	250		8620	197	5880	29.7	87.6	114	66.3	56.7	659	201	374			215	807	922	53.9	679	2140	2100		45.5	27.3	27.7	4.6	153.0	65.9	14.4	68.8	15.9	22.1		-4.6	6.0	0.8	19.8	82.6	-10.8	116.0	38.5	4.4	81.7	-7.1			-17.0	-6.5	26.5	19.6	-6.6	-17.7	-19.9
0.02	0.01	0.03	Alanine-3-13C-Experiment	12			42.6	93.0	37.0	787	455	477	66.4	200	1160	223		7120	160	5780	74.4	34.2	121	60.1	47.9	753	218	393			221	703	869	43.7	794	1230	1850		104.0	80.0	110.0	58.2	305.0	145.0	70.0	166.0	67.0	74.6		31.0	60.3	40.9	77.7	356.0	-14.5	312.0	162.0	39.4	251.0	131.0			-16.4	15.9	172.0	108.0	21.5	-17.2	-21.5
0.02	0.01	0.03	Alanine-3-13C-Experiment	24			60.7	129.0	52.7	1010	609	626	83.1	231	1300	291		9340	226	6720	40.1	55.5	124	80.8	59.6	764	239	450			182	888	1160	56.6	700	2120	1920		128.0	110.0	228.0	116.0	374.0	178.0	137.0	228.0	105.0	109.0		87.5	143.1	88.4	83.8	542.0	-11.4	321.0	194.0	76.3	409.0	196.0			-17.4	29.2	382.0	264.0	60.9	-18.3	-19.6
0.02	0.01	0.03	Alanine-3-13C-Experiment	36			46.4	82.6	68.9	720	482	465	52.6	168	952	314		7270	466	5460	145.0	50.2	108	66.7	43.4	743	187	352			197	776	983	59.2	652	1660	1410		115.0	115.0	241.0	122.0	394.0	196.0	152.0	238.0	110.0	122.0		98.1	184.6	94.1	96.3	653.0	-12.9	426.0	217.0	80.4	441.0	200.0			-14.5	36.5	427.0	390.0	47.7	-17.0	-19.6
0.02	0.01	0.03	Valine-2-13C-Experiment		Background	38.3	57.8	106.0	50.0	1380	615	669	114.0	323	1830	290	1280	14500	264	10200	18.4	63.4	119	83.3	57.6	1020	325	573				1100	1320	63.9	823	2600	2500	-23.2	-23.1	-21.0	-13.9	-17.5	-20.3	-17.1	-21.9	-17.5	-18.8	-19.1	-24.1	-18.0	-35.6	-20.0	-9.9	-18.3	-25.3	-25.4	-15.8	-19.7	-27.3	-17.6				-18.5	-21.5	-35.1	-23.8	-18.3	-19.8
0.02	0.01	0.03	Valine-2-13C-Experiment	0		36.7	50.9	103.0	43.1	1240	542	610	103.0	281	1580	271	1300	12900	240	8510	17.4	65.3	100	73.9	56.1	923	305	500				990	1230	56.0	802	2200	1840	-23.1	-22.5	-17.7	-14.6	-17.9	-19.0	-16.6	-22.4	-15.7	-19.1	-6.6	-23.3	-18.6	-37.4	-19.1	-4.5	-3.4	-23.1	-20.4	-9.6	-19.6	-25.6	-16.7				-18.9	-21.7	-34.3	-25.2	-18.2	-19.8
0.02	0.01	0.03	Valine-2-13C-Experiment	3		46.4	69.8	133.0	62.4	1430	643	794	127.0	309	1840	279	1070	14300	593	10400	14.1	72.8	111	90.8	64.4	1080	321	575				1240	1360	71.4	1110	1730	1600	-4.6	-19.0	81.3	-13.3	-11.4	8.8	-10.7	-17.5	-14.2	-17.6	56.2	-22.0	-17.8	-34.1	-15.9	16.5	0.4	-21.5	4.3	-0.3	-19.2	-18.8	-14.5				-16.4	-18.0	-34.5	-21.6	-17.5	-19.3
0.02	0.01	0.03	Valine-2-13C-Experiment	6		58.8	81.3	145.0	65.8	1530	709	805	138.0	336	1950	280	977	15200	602	11100	16.5	81.2	119	99.3	62.0	1100	351	603				1240	1400	77.4	1260	1400	1100	5.2	-15.3	164.0	-5.9	-4.4	33.7	-5.1	-14.0	-7.8	-17.1	122.0	-21.9	-17.0	-32.3	-13.1	35.0	17.3	-20.3	6.0	5.1	-18.3	-16.0	-11.2				-13.6	-14.5	-35.9	-18.2	-16.9	-18.5
0.02	0.01	0.03	Valine-2-13C-Experiment	12		49.0	65.8	147.0	77.7	1310	719	795	129.0	337	1770	311	1180	13700	606	9730	19.9	77.9	128	103.0	70.4	1040	339	641				1200	1410	73.3	951	1380	1140	37.0	-13.0	360.0	5.6	9.4	90.6	7.5	-6.3	-5.8	-15.7	240.0	-20.3	-15.7	-24.5	-5.7	42.2	58.3	-19.9	52.2	10.9	-18.3	-11.6	-6.2				-10.3	-3.4	-5.4	-11.5	-17.8	-19.0
0.02	0.01	0.03	Valine-2-13C-Experiment	24		74.7	87.3	177.0	105.0	1750	878	919	145.0	354	2140	363	1300	17100	668	11500	15.6	87.8	128	107.0	65.5	1250	381	579				1360	1500	80.2	1010	2170	1900	66.6	-10.8	684.0	22.1	32.6	190.0	27.8	8.3	6.9	-12.5	428.0	-18.1	-4.9	0.5	10.2	95.1	187.0	-12.1	73.1	25.8	-14.0	-0.2	-2.0				-1.6	55.8	7.9	-2.1	-17.0	-18.8
0.02	0.01	0.03	Valine-2-13C-Experiment	36		48.3	57.3	152.0	95.4	1840	737	866	124.0	284	2160	602	948	13300	614	13400	19.8	111.0	109	121.0	80.9	999	286	716				1420	1340	87.1	3580	1690	1390	93.8	-11.9	643.0	35.3	29.3	229.0	36.0	15.0	11.8	-10.7	345.0	-11.1	14.8	31.0	13.6	268.0	235.0	-11.3	91.3	24.7	-12.2	7.8	5.1				0.9	160.0	69.5	-17.4	-16.0	-19.1
0.02	0.01	0.03	Leucine-3-13C-Experiment		Background	44.2	70.6	127.0	33.9	1720	595	688	169.0		2220	332		20900	267	13000	21.5	77.1	132	87.9	60.8		411	736	95.4	301		1530	1340	64.9		2310	2970	-23.5	-23.1	-19.5	-16.7	-17.8	-19.7	-19.7	-23.7		-19.1	-18.4		-14.8	-38.0	-17.8	-9.9	-14.8	-25.1	-25.1	-17.8		-24.4	-18.5	-12.0	-15.5		-19.2	-20.2	-32.4		-16.1	-18.3
0.02	0.01	0.03	Leucine-3-13C-Experiment	0		43.9	63.4		31.1	1480	598	702	178.0		1800	313		14700	264	10400	22.8	67.8	139	81.1	89.2		437	662	101.0	334		1090	1000	61.4		1540	1450	-21.5	-22.7		-15.8	-19.0	-17.0	-16.9	-25.7		-19.2	-6.6		-14.7	-35.8	-18.1	-8.9	-14.3	-24.5	-21.0	-1.4		-20.9	-20.1	-12.9	-16.3		-17.9	-22.3	-33.5		-17.1	-18.4
0.02	0.01	0.03	Leucine-3-13C-Experiment	3		46.1	63.7	122.0	36.8	1320	546	619	149.0		1720	329		10700	244	9780	42.8	54.9	119	74.4	69.2		403	649	86.0	251		857	807	63.1		983	832	61.5	-18.1	-19.3	-16.7	-17.9	108.0	-5.8	-21.8		-19.8	-3.7		-14.2	-34.6	-17.8	-6.6	4.2	-23.3	83.0	-1.9		-21.2	-18.3	-12.7	-17.3		-17.5	-15.6	-30.4		-16.9	-18.4
0.02	0.01	0.03	Leucine-3-13C-Experiment	6		79.3	107.0	120.0	90.7	3080	1030	1180	324.0		3840	493		34700	418	21000	39.3	83.8	222	130.0	160.0		702	1200	201.0	422		2410	2420	105.3		4080	4640	135.0	-17.1	-19.0	-17.5	-17.5	215.0	1.6	-22.0		-18.9	-4.3		-13.9	-33.0	-17.6	-6.7	24.8	-15.0	137.0	1.4		-21.6	-18.1	-10.8	-16.2		-17.9	-11.0	-25.6		-17.2	-18.7
0.02	0.01	0.03	Leucine-3-13C-Experiment	12		61.7	83.2	214.0	26.8	1840	676	706	189.0		2230	307		21600	273	12100	15.7	54.9	154	79.6	86.4		483	683	90.6	280		1410	1230	63.3		2150	2400	309.0	-16.0	-18.6	-15.1	-16.2	447.0	29.6	-11.4		-16.1	-0.1		-12.1	-26.1	-15.7	12.2	271.0	8.9	313.0	2.6		-16.6	-14.9	-10.1	-16.4		-16.4	2.0	-22.2		-17.1	-18.0
0.02	0.01	0.03	Leucine-3-13C-Experiment	24		53.7	78.5	143.0	51.1	1690	680	669	164.0		2080	312		19200	257	11600	15.0	63.5	137	83.0	74.4		416	688	83.1	242		1310	1160	62.5		2020	2150	606.0	-13.1	-13.8	0.3	-14.3	816.0	72.0	9.6		-14.3	11.7		-5.3	-24.9	-8.2	54.8	741.0	38.5	622.0	9.0		-14.9	-10.9	-10.4	-11.8		-12.6	63.2	-20.7		-17.0	-18.1
0.02	0.01	0.03	Leucine-3-13C-Experiment	36		56.5	52.8	135.0	35.5	1610	678	640	149.0		1840	372		17700	287	10200	14.6	65.1	144	78.7	63.1		396	606	73.8	229		1290	1180	72.9		2000	2130	766.0	-11.6	-4.9	30.9	-6.2	1110.0	96.7	24.6		-11.8	18.6		15.9	-2.2	7.6	56.0	987.0	27.5	1070.0	20.1		-1.2	-4.8	0.9	-6.1		-9.3	185.0	81.5		-16.2	-18.6
0.02	0.01	0.03	Leucine-1-13C-Experiment		Background	53.5	66.8	156.0	68.8	1560	701	794	133.0	348		329		16400		10800	24.6	77.7	142	80.6	69.0		356	634					1510	73.6		2620	2170	-23.4	-22.2	-20.0	-15.8	-20.4	-20.3	-18.3	-20.8	-15.5		-18.8		-18.1		-20.0	-9.7	-15.7	-24.2	-25.7	-17.8		-26.0	-21.7					-23.6	-36.4		-16.9	-18.4
0.02	0.01	0.03	Leucine-1-13C-Experiment	0		72.6	85.6	173.0	66.3	1680	735	807	144.0	413		363		17400		11200	29.2	79.5	124	76.4	71.7		393	658					1610	77.1		2890	2660	-21.2	-20.4	-19.4	-15.6	-19.5	-18.8	-18.2	-21.6	-17.3		-7.9		-17.8		-19.6	-9.6	-15.4	-19.6	-19.2	-5.1		-22.7	-22.7					-22.7	-33.9		-17.8	-19.0
0.02	0.01	0.03	Leucine-1-13C-Experiment	3		68.7	82.7	161.0	70.1	1590	722	780	127.0	377		333		16300		10600	21.7	78.3	144	89.6	72.0		393	648					1530	69.5		2570	2390	-20.1	-20.1	-19.3	-14.6	-19.2	-18.8	-17.5	-21.1	-16.4		-9.8		-17.0		-19.2	-6.3	-17.7	-14.9	-19.1	-11.4		-14.8	-22.5					-21.3	-31.0		-18.1	-19.4
0.02	0.01	0.03	Leucine-1-13C-Experiment	6		62.8	83.3	159.0	67.7	1440	666	711	122.0	331		310		14500		9490	32.1	73.7	124	81.7	68.5		332	577					1440	65.6		2550	2400	-19.0	-19.3	-18.9	-14.9	-19.0	-19.0	-17.5	-16.2	-15.9		-8.7		-16.9		-19.2	-3.6	-18.0	-15.0	-18.5	-10.4		-6.7	-21.2					-21.3	-29.8		-18.2	-19.7
0.02	0.01	0.03	Leucine-1-13C-Experiment	12		44.1	51.7	138.0	59.8	1380	688	709	125.0	333		287		14900		10100	20.0	80.1	122	90.2	62.4		362	612					1440	72.9		2440	1940	-19.2	-17.9	-18.4	-14.4	-18.2	-17.8	-15.7	-14.7	-14.1		-8.1		-17.0		-19.0	9.1	-14.7	-17.2	-16.0	-6.3		-5.4	-18.8					-21.0	-29.3		-17.9	-19.2
0.02	0.01	0.03	Leucine-1-13C-Experiment	24		48.8	55.4	135.0	64.4	1290	705	718	114.0	270		271		11600		8600	20.0	76.7	122	79.7	58.9		320	568					1350	72.1		2580	2050	-17.9	-17.6	-18.4	-13.9	-16.8	-12.5	-13.5	-14.4	-13.5		-6.7		-15.8		-18.6	13.5	-11.3	-16.0	-10.0	-4.3		-6.3	-16.6					-20.3	-27.9		-17.9	-19.5
0.02	0.01	0.03	Leucine-1-13C-Experiment	36		47.3	49.4	161.0	95.6	1670	1070	1020	179.0	387		379		20700		14900	30.4	117.0	164	124.0	87.3		454	754					2240	109.0		2540	1920	-16.1	-17.2	-12.3	-10.6	-16.4	-8.4	-9.6	-12.5	-12.6		-5.6		-14.1		-15.7	22.4	-3.9	-16.5	-9.0	-4.8		-9.2	-14.1					-11.1	-13.3		-17.5	-18.8