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Henkel, Susann; Kasten, Sabine; Hartmann, Jan; Silva Busso, A; Staubwasser, Michael (2018): Pore water geochemistry of sediment core Maxwell_Bay_STA05 [dataset]. Alfred Wegener Institute, Helmholtz Centre for Polar and Marine Research, Bremerhaven, PANGAEA, https://doi.org/10.1594/PANGAEA.890295, In supplement to: Henkel, S et al. (2018): Iron cycling and stable Fe isotope fractionation in Antarctic shelf sediments, King George Island. Geochimica et Cosmochimica Acta, https://doi.org/10.1016/j.gca.2018.06.042

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Further details:
Lohan, Maeve C; Aguilar-Islas, Ana M; Franks, Robert P; Bruland, Kenneth W (2005): Determination of iron and copper in seawater at pH 1.7 with a new commercially available chelating resin, NTA Superflow. Analytica Chimica Acta, 530(1), 121-129, https://doi.org/10.1016/j.aca.2004.09.005
Schoenberg, Ronny; von Blanckenburg, Friedhelm (2005): An assessment of the accuracy of stable Fe isotope ratio measurements on samples with organic and inorganic matrices by high-resolution multicollector ICP-MS. International Journal of Mass Spectrometry, 242(2-3), 257-272, https://doi.org/10.1016/j.ijms.2004.11.025
Seeberg-Elverfeldt, Jens; Schlüter, Michael; Feseker, Tomas; Kölling, Martin (2005): Rhizon sampling of pore waters near the sediment/water interface of aquatic systems. Limnology and Oceanography: Methods, 3, 361-371, https://doi.org/10.4319/lom.2005.3.361
Stookey, Lawrence L (1970): Ferrozine - A new spectrophotometric reagent for iron. Analytical Chemistry, 42, 779-781, https://doi.org/10.1021/ac60289a016
Funding:
German Research Foundation (DFG), grant/award no. 5472008: Priority Programme 1158 Antarctic Research with Comparable Investigations in Arctic Sea Ice Areas
Coverage:
Latitude: -62.222720 * Longitude: -58.930040
Date/Time Start: 2012-01-31T00:00:00 * Date/Time End: 2012-01-31T00:00:00
Minimum DEPTH, sediment/rock: -0.01 m * Maximum DEPTH, sediment/rock: 0.14 m
Event(s):
Maxwell_Bay_STA05 * Latitude: -62.222720 * Longitude: -58.930040 * Date/Time: 2012-01-31T00:00:00 * Elevation: -44.0 m * Location: Maxwell Bay, King George Island, Antarctic Peninsula * Method/Device: Gravity corer, UWITEC (GCUWI) * Comment: Elevation error ±1.5 m (tidal range)
Comment:
Methods:
Sampling:
•Rhizon technique (Seeberg-Elverfeldt et al. 2005)
SO42-
•Ion chromatography (Metrohm IC Net 2.3)
Fe2+
•Ferrozine method (Stookey 1970)
NH4+
•conductometrically
Alkalinity
•Titration with HCl
δ56Fepw
•Removal of salt matrix by column chromatography (NTA Superflow columns, Qiagen) (Lohan et al. 2005)
•Column separation using the Dowex 1X8 resin
•Isotope analysis on a ThermoFinnigan Neptune Multicollector-ICP-MS (ESI Apex-Q desolvator, standard-sample bracketing method with IRMM-014) (Schoenberg and von Blanckenburg 2005)
Parameter(s):
#NameShort NameUnitPrincipal InvestigatorMethod/DeviceComment
1CoreCoreHenkel, Susann
2DEPTH, sediment/rockDepth sedmHenkel, SusannGeocode
3Sulfate[SO4]2-mmol/lHenkel, SusannIon chromatography (Metrohm IC Net 2.3)
4Iron 2+Fe2+µmol/lHenkel, SusannIron, colorimetric, Ferrozine (Stookey, 1970)
5Alkalinity, totalATmmol(eq)/lHenkel, SusannTitration with HCl
6Ammonium[NH4]+µmol/lHenkel, SusannConductometry
7CommentCommentHenkel, Susann
Size:
62 data points

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