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Felden, Janine; Boetius, Antje (2013): Pore water geochemistry of Håkon Mosby mud volcano sediments measured at station PS74/169-1_PUC-15 (Sample 1, new flow surface) [dataset]. Max-Planck-Institut für Marine Mikrobiologie, PANGAEA, https://doi.org/10.1594/PANGAEA.810919, In supplement to: Ruff, S Emil; Felden, Janine; Gruber-Vodicka, Harald R; Marcon, Yann; Knittel, Katrin; Ramette, Alban; Boetius, Antje (2018): In situ development of a methanotrophic microbiome in deep-sea sediments. The ISME Journal, https://doi.org/10.1038/s41396-018-0263-1

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Abstract:
Pore water and turnover rates were determined for surface sediment cores obtained in 2009 and 2010. The pore water was extracted with Rhizons (Rhizon CSS: length 5 cm, pore diameter 0.15 µm; Rhizosphere Research Products, Wageningen, Netherlands) in 1 cm-resolution and immediately fixed in 5% zinc acetate (ZnAc) solution for sulfate, and sulfide analyses. The samples were diluted, filtered and the concentrations measured with non-suppressed anion exchange chromatography (Waters IC-Pak anion exchange column, waters 430 conductivity detector). The total sulfide concentrations (H2S + HS- + S**2-) were determined using the diamine complexation method (doi:10.4319/lo.1969.14.3.0454). Samples for dissolved inorganic carbon (DIC) and alkalinity measurements were preserved by adding 2 µl saturated mercury chloride (HgCl2) solution and stored headspace-free in gas-tight glass vials. DIC and alkalinity were measured using the flow injection method (detector VWR scientific model 1054) (doi:10.4319/lo.1992.37.5.1113). Dissolved sulfide was eliminated prior to the DIC measurement by adding 0.5 M molybdate solution (doi:10.4319/lo.1995.40.5.1011). Nutrient subsamples (10 - 15 ml) were stored at – 20 °C prior to concentration measurements with a Skalar Continuous-Flow Analyzer (doi:10.1002/9783527613984).
Funding:
Seventh Framework Programme (FP7), grant/award no. 226354: Hotspot Ecosystem Research and Mans Impact On European Seas
Sixth Framework Programme (FP6), grant/award no. 36851: European Seafloor Observatory Network
Coverage:
Latitude: 72.005000 * Longitude: 14.726402
Date/Time Start: 2009-07-23T18:22:43 * Date/Time End: 2009-07-23T18:22:43
Minimum DEPTH, sediment/rock: 0.005 m * Maximum DEPTH, sediment/rock: 0.110 m
Event(s):
PS74/169-1_PUC-15 * Latitude: 72.005000 * Longitude: 14.726402 * Date/Time: 2009-07-23T18:22:43 * Elevation: -1261.0 m * Location: Håkon Mosby Mud Volcano * Campaign: ARK-XXIV/2 (PS74) * Basis: Polarstern * Method/Device: Push corer (PUC)
Parameter(s):
#NameShort NameUnitPrincipal InvestigatorMethod/DeviceComment
DEPTH, sediment/rockDepth sedmGeocode
SulfideS2-µmol/lFelden, JaninePhotometer, methylene blue (Cline 1969)
Sulfate[SO4]2-mmol/lFelden, JanineIon chromatography
Carbon, inorganic, dissolvedDICmmol/lFelden, JanineFlow injection analysis (Hall and Aller 1992)CO2 + HCO3- + CO32-
Alkalinity, totalATmmol(eq)/lFelden, JanineTwo-point titration (Edmond 1970)
SilicateSi(OH)4µmol/lFelden, JanineSeawater analysis after Grasshoff et al., 1983 (Verlag Chemie GmbH Weinheim)
Phosphate[PO4]3-µmol/lFelden, JanineSeawater analysis after Grasshoff et al., 1983 (Verlag Chemie GmbH Weinheim)
Ammonium[NH4]+µmol/lFelden, JanineSeawater analysis after Grasshoff et al., 1983 (Verlag Chemie GmbH Weinheim)
Size:
74 data points

Data

Download dataset as tab-delimited text — use the following character encoding:


Depth sed [m]

S2- [µmol/l]

[SO4]2- [mmol/l]

DIC [mmol/l]

AT [mmol(eq)/l]

Si(OH)4 [µmol/l]

[PO4]3- [µmol/l]

[NH4]+ [µmol/l]
0.0053626.200.55.8281642
0.0153523.350.89.6521803
0.0253618.921.012.714011722
0.0353613.801.414.920212169
0.0453610.271.613.921812447
0.055396.941.716.036333040
0.065374.402.020.334933186
0.075393.002.020.333043223
0.085392.482.226.532543144
0.095371.992.228.332133184
0.110631.722.327.0