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Klapp, Stephan A; Klein, Helmut; Kuhs, Werner F (2007): (Table 1) Crystal sizes of measured samples [dataset]. PANGAEA, https://doi.org/10.1594/PANGAEA.771920, Supplement to: Klapp, SA et al. (2007): First determination of gas hydrate crystallite size distributions using high-energy synchrotron radiation. Geophysical Research Letters, 34, L13608, https://doi.org/10.1029/2006GL029134

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Abstract:
Due to experimental difficulties grain size distributions of gas hydrate crystallites are largely unknown in natural samples. For the first time, we were able to determine grain size distributions of six natural gas hydrates for samples retrieved from the Gulf of Mexico and from Hydrate Ridge offshore Oregon from varying depths. High-energy synchrotron radiation provides high photon fluxes as well as high penetration depth and thus allows for investigation of bulk sediment samples. The gas hydrate crystallites appear to be (log-) normally distributed in the natural samples and to be of roughly globular shape. The mean grain sizes are in the range from 300–600 µm with a tendency for bigger grains to occur in greater depth, possibly indicating a difference in the formation age. Laboratory produced methane hydrate, starting from ice and aged for 3 weeks, shows half a log-normal curve with a mean value of ~40 µm. This one order-of-magnitude smaller grain sizes suggests that care must be taken when transposing grain-size sensitive (petro-)physical data from laboratory-made gas hydrates to natural settings.
Project(s):
Coverage:
Median Latitude: 41.214804 * Median Longitude: -118.421848 * South-bound Latitude: 27.782750 * West-bound Longitude: -125.152500 * North-bound Latitude: 44.577650 * East-bound Longitude: -91.507810
Date/Time Start: 2002-07-25T13:30:00 * Date/Time End: 2003-11-06T17:24:00
Minimum DEPTH, sediment/rock: 1.50 m * Maximum DEPTH, sediment/rock: 100.89 m
Event(s):
204-1247B  * Latitude: 44.577650 * Longitude: -125.151280 * Date/Time Start: 2002-08-22T06:45:00 * Date/Time End: 2002-08-24T19:15:00 * Elevation: -834.3 m * Penetration: 220 m * Recovery: 211.98 m * Location: North Pacific Ocean * Campaign: Leg204 * Basis: Joides Resolution * Method/Device: Drilling/drill rig (DRILL) * Comment: 27 cores; 217 m cored; 3 m drilled; 97.7 % recovery
204-1248C  * Latitude: 44.574230 * Longitude: -125.152500 * Date/Time Start: 2002-08-01T13:45:00 * Date/Time End: 2002-08-02T12:30:00 * Elevation: -829.6 m * Penetration: 149 m * Recovery: 101.44 m * Location: North Pacific Ocean * Campaign: Leg204 * Basis: Joides Resolution * Method/Device: Drilling/drill rig (DRILL) * Comment: 17 cores; 149 m cored; 0 m drilled; 68.1 % recovery
204-1249C  * Latitude: 44.570610 * Longitude: -125.147350 * Date/Time Start: 2002-07-25T13:30:00 * Date/Time End: 2002-07-26T11:45:00 * Elevation: -778.4 m * Penetration: 90 m * Recovery: 58.97 m * Location: North Pacific Ocean * Campaign: Leg204 * Basis: Joides Resolution * Method/Device: Drilling/drill rig (DRILL) * Comment: 14 cores; 88.5 m cored; 1.5 m drilled; 66.6 % recovery
Parameter(s):
#NameShort NameUnitPrincipal InvestigatorMethod/DeviceComment
Event labelEvent
Elevation of eventElevationm
Latitude of eventLatitude
Longitude of eventLongitude
Sample code/labelSample labelKlapp, Stephan A
DEPTH, sediment/rockDepth sedmGeocode
Depth commentDepth commKlapp, Stephan A
Grain size, meanGrain size meanµmKlapp, Stephan ALocation scan method
Standard deviationStd dev±Klapp, Stephan A
Size:
26 data points

Data

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Event

Elevation [m]

Latitude

Longitude

Sample label

Depth sed [m]

Depth comm

Grain size mean [µm]

Std dev [±]
204-1247B -83444.577650-125.151280204-1247B-12H-2, 41-5193.01592374
204-1249C -77844.570610-125.147350204-1249C-1H-CC, 0-101.50373134
204-1248C -83044.574230-125.152500204-248C-8H-6, 68-8774.4636179
204-1248C-83044.574230-125.152500204-1248C 11H-5 (no tilt)100.89517176
204-1248C-83044.574230-125.152500204-1248C 11H-5 (90° tilted)100.89569342
204-1250C -79644.568780-125.150300204-1250C 2H-CC 0-1 cm5.06451132
SO174/2_157-2 -54727.782750-91.507810Bush Hill, TVG 10 GH 1sea floor301114
CH4-Hydratesynthetic4324